Technology Process of C19H23Cl3N2O5S2
There total 7 articles about C19H23Cl3N2O5S2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triethyl borane; oxygen; N-ethylpiperidinium hypophosphite;
In
1,4-dioxane; hexane;
at 73 ℃;
for 2h;
Air atmosphere;
DOI:10.1016/j.tetlet.2011.10.093
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: triethylamine / dichloromethane / -78 - 20 °C
2.1: 2,2'-azobis(isobutyronitrile); bromine / 1,2-dichloro-ethane / 3 h / Reflux
2.2: 1.08 h / -78 - 20 °C
3.1: 1 h / 190 °C / Neat (no solvent)
4.1: triethyl borane; oxygen; N-ethylpiperidinium hypophosphite / 1,4-dioxane; hexane / 2 h / 73 °C / Air atmosphere
With
2,2'-azobis(isobutyronitrile); triethyl borane; bromine; oxygen; triethylamine; N-ethylpiperidinium hypophosphite;
In
1,4-dioxane; hexane; dichloromethane; 1,2-dichloro-ethane;
3.1: Michael addition;
DOI:10.1016/j.tetlet.2011.10.093
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 2,2'-azobis(isobutyronitrile); bromine / 1,2-dichloro-ethane / 3 h / Reflux
1.2: 1.08 h / -78 - 20 °C
2.1: 1 h / 190 °C / Neat (no solvent)
3.1: triethyl borane; oxygen; N-ethylpiperidinium hypophosphite / 1,4-dioxane; hexane / 2 h / 73 °C / Air atmosphere
With
2,2'-azobis(isobutyronitrile); triethyl borane; bromine; oxygen; N-ethylpiperidinium hypophosphite;
In
1,4-dioxane; hexane; 1,2-dichloro-ethane;
2.1: Michael addition;
DOI:10.1016/j.tetlet.2011.10.093
![1-bromo-2-[(4-diethylsulfamoylphenyl)methylamino]ethanesulfonic acid 2,4,6-trichlorophenyl ester](/Databaselist/images/loading.webp)
