C₂₈H₃₃IN₂O₈

Base Information

Chemical Name:C₂₈H₃₃IN₂O₈
CAS No.:1315454-73-9
Molecular Formula:C₂₈H₃₃IN₂O₈
Molecular Weight:652.483
Hs Code.:

C<sub>28</sub>H<sub>33</sub>IN<sub>2</sub>O<sub>8</sub>

Synonyms:C₂₈H₃₃IN₂O₈

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Chemical Property of C₂₈H₃₃IN₂O₈

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Technology Process of C₂₈H₃₃IN₂O₈

There total 17 articles about C₂₈H₃₃IN₂O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1016976-38-7
C₂₆H₃₁IN₂O₆

: 79-22-1
methyl chloroformate

: 1315454-73-9
C₂₈H₃₃IN₂O₈

Guidance literature:: With dmap; potassium carbonate; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1002/chem.201003489

Reference yield:

: 885703-19-5
(3S,4S)-4-N-phthalimido-1,5-hexadiene-3-ol

: 1315454-73-9
C₂₈H₃₃IN₂O₈

Guidance literature:: Multi-step reaction with 13 steps

1: 1H-imidazole / N,N-dimethyl-formamide / 11 h / 20 °C / Inert atmosphere

2: osmium(VIII) oxide; (8a,9R,8′′′a,9′′′R)-9,9′-[(2,5-diphenylpyrimidine-4,6-diyl)bis(oxy)]bis(6′-methoxy-10,11-dihydrocinchonan); methanesulfonamide; sodium hydrogencarbonate; potassium carbonate; potassium hexacyanoferrate(III) / water; tert-butyl alcohol / 6 h / 5 °C / Inert atmosphere

3: nitrogen; methylamine / water / 1 h / 50 °C / 10 Torr / Inert atmosphere

4: sodium hydrogencarbonate / ethyl acetate / 1.5 h / Inert atmosphere

5: dmap; triethylamine; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.03 h / 0 - 20 °C / Inert atmosphere

6: dichloromethane / 1 h / -40 °C / Inert atmosphere

7: caesium carbonate / N,N-dimethyl-formamide / 4 h / 60 °C / Inert atmosphere

8: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 2 h / Inert atmosphere

9: Dess-Martin periodane / dichloromethane / 1.5 h / 20 °C / Inert atmosphere

10: acetic acid / chloroform / 12 h / 20 °C / Molecular sieve; Inert atmosphere

11: sodium cyanoborohydride / tetrahydrofuran / 2 h / Inert atmosphere

12: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

13: dmap; potassium carbonate / dichloromethane / 20 °C / Inert atmosphere

With 1H-imidazole; dmap; osmium(VIII) oxide; (8a,9R,8′′′a,9′′′R)-9,9′-[(2,5-diphenylpyrimidine-4,6-diyl)bis(oxy)]bis(6′-methoxy-10,11-dihydrocinchonan); methanesulfonamide; nitrogen; tetrabutyl ammonium fluoride; sodium cyanoborohydride; sodium hydrogencarbonate; potassium carbonate; caesium carbonate; Dess-Martin periodane; acetic acid; triethylamine; N-ethyl-N,N-diisopropylamine; methylamine; potassium hexacyanoferrate(III); In tetrahydrofuran; dichloromethane; chloroform; water; ethyl acetate; N,N-dimethyl-formamide; tert-butyl alcohol;
DOI:10.1002/chem.201003489

Reference yield:

: 1016976-13-8
3-benzyloxy-4-iodo-5-nitrobenzaldehyde

: 1315454-73-9
C₂₈H₃₃IN₂O₈

Guidance literature:: Multi-step reaction with 6 steps

1: N-iodo-succinimide; potassium carbonate / acetonitrile / 12 h / 5 °C / Inert atmosphere; Darkness

2: iron; acetic acid / tetrahydrofuran; methanol / 3.5 h / 20 °C / Inert atmosphere

3: acetic acid / chloroform / 12 h / 20 °C / Molecular sieve; Inert atmosphere

4: sodium cyanoborohydride / tetrahydrofuran / 2 h / Inert atmosphere

5: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

6: dmap; potassium carbonate / dichloromethane / 20 °C / Inert atmosphere

With dmap; N-iodo-succinimide; tetrabutyl ammonium fluoride; iron; sodium cyanoborohydride; potassium carbonate; acetic acid; In tetrahydrofuran; methanol; dichloromethane; chloroform; acetonitrile;
DOI:10.1002/chem.201003489