N'-[1-(4-Hydroxy-phenyl)-meth-(E)-ylidene]-hydrazinecarboxylic acid benzyl ester

Base Information

Chemical Name:N'-[1-(4-Hydroxy-phenyl)-meth-(E)-ylidene]-hydrazinecarboxylic acid benzyl ester
CAS No.:936911-77-2
Molecular Formula:C₁₅H₁₄N₂O₃
Molecular Weight:270.288
Hs Code.:

Synonyms:N'-[1-(4-Hydroxy-phenyl)-meth-(E)-ylidene]-hydrazinecarboxylic acid benzyl ester

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Chemical Property of N'-[1-(4-Hydroxy-phenyl)-meth-(E)-ylidene]-hydrazinecarboxylic acid benzyl ester

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Technology Process of N'-[1-(4-Hydroxy-phenyl)-meth-(E)-ylidene]-hydrazinecarboxylic acid benzyl ester

There total 1 articles about N'-[1-(4-Hydroxy-phenyl)-meth-(E)-ylidene]-hydrazinecarboxylic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 5331-43-1
N-benzyloxycarbonyl-hydrazine

: 123-08-0,65581-83-1
4-hydroxy-benzaldehyde

: 936911-77-2
N'-[1-(4-Hydroxy-phenyl)-meth-(E)-ylidene]-hydrazinecarboxylic acid benzyl ester

Guidance literature:: With acetic acid; In ethanol; at 20 ℃;
DOI:10.1021/jm061477+

Reference yield:

: 936911-77-2
N'-[1-(4-Hydroxy-phenyl)-meth-(E)-ylidene]-hydrazinecarboxylic acid benzyl ester

: N'-(4-Hydroxy-benzyl)-hydrazinecarboxylic acid benzyl ester

Guidance literature:: With sodium cyanoborohydride; In tetrahydrofuran; acetic acid; Ambient temperature;
DOI:10.1016/0223-5234(96)88312-7

Reference yield:

: 936911-77-2
N'-[1-(4-Hydroxy-phenyl)-meth-(E)-ylidene]-hydrazinecarboxylic acid benzyl ester

: N-benzyloxycarbonyl-α-azatyrosyl-1-aminopropan-2-one

Guidance literature:: Multi-step reaction with 4 steps

1: NaBH₃CN / tetrahydrofuran; acetic acid / Ambient temperature

2: 0.5M aq. NaHCO₃ / CHCl₃; ethyl acetate / 0.5 h / Ambient temperature

3: dioxane / 22 h / 80 °C

4: 1M aq. oxalic acid / tetrahydrofuran / 5 h / Ambient temperature

With oxalic acid; sodium cyanoborohydride; sodium hydrogencarbonate; In tetrahydrofuran; 1,4-dioxane; chloroform; acetic acid; ethyl acetate;
DOI:10.1016/0223-5234(96)88312-7