(4,4',5,5'-tetrachloro-1'H-1,3'-bipyrrole-2,2'-diyl)bis((2-acetoxyphenyl)methanone)

Base Information

Chemical Name:(4,4',5,5'-tetrachloro-1'H-1,3'-bipyrrole-2,2'-diyl)bis((2-acetoxyphenyl)methanone)
CAS No.:1305334-97-7
Molecular Formula:C₂₆H₁₆Cl₄N₂O₆
Molecular Weight:594.235
Hs Code.:

Synonyms:(4,4',5,5'-tetrachloro-1'H-1,3'-bipyrrole-2,2'-diyl)bis((2-acetoxyphenyl)methanone)

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Chemical Property of (4,4',5,5'-tetrachloro-1'H-1,3'-bipyrrole-2,2'-diyl)bis((2-acetoxyphenyl)methanone)

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Technology Process of (4,4',5,5'-tetrachloro-1'H-1,3'-bipyrrole-2,2'-diyl)bis((2-acetoxyphenyl)methanone)

There total 9 articles about (4,4',5,5'-tetrachloro-1'H-1,3'-bipyrrole-2,2'-diyl)bis((2-acetoxyphenyl)methanone) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 1010732-14-5,1227962-62-0,1306747-26-1
[4,5-dichloro-1-[4,5-dichloro-2-(2-hydroxybenzoyl)-1H-pyrrol-3-yl]pyrrol-2-yl]-(2-hydroxyphenyl)methanone

: 108-24-7
acetic anhydride

: 1305334-97-7
(4,4',5,5'-tetrachloro-1'H-1,3'-bipyrrole-2,2'-diyl)bis((2-acetoxyphenyl)methanone)

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 25 ℃; for 12h; Inert atmosphere;
DOI:10.1016/j.tetlet.2010.09.059

Reference yield: 62.0%

: marinopyrrole A

: 108-24-7
acetic anhydride

: 1305334-97-7
(4,4',5,5'-tetrachloro-1'H-1,3'-bipyrrole-2,2'-diyl)bis((2-acetoxyphenyl)methanone)

Guidance literature:: With pyridine; dmap; at 20 ℃;
DOI:10.1021/jo1002054

Reference yield:

: 1227869-59-1
1'H-1,3'-bipyrrole-2,2'-diylbis[(2-methoxyphenyl)methanone]

: 1305334-97-7
(4,4',5,5'-tetrachloro-1'H-1,3'-bipyrrole-2,2'-diyl)bis((2-acetoxyphenyl)methanone)

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuryl dichloride / dichloromethane / 1 h / 0 °C / Inert atmosphere

2: boron tribromide / dichloromethane / 1 h / 0 °C / Inert atmosphere

3: dmap; triethylamine / dichloromethane / 12 h / 25 °C / Inert atmosphere

With dmap; sulfuryl dichloride; boron tribromide; triethylamine; In dichloromethane;
DOI:10.1016/j.tetlet.2010.09.059