6'-azido-4',5'-dehydro-3',4'-dideoxy-6,3',2'',5'',3''',4'''-hexa-O-methoxycarbonyl-per-N-Cbz-neomycin

Base Information

Chemical Name:6'-azido-4',5'-dehydro-3',4'-dideoxy-6,3',2'',5'',3''',4'''-hexa-O-methoxycarbonyl-per-N-Cbz-neomycin
CAS No.:1284216-89-2
Molecular Formula:C₇₃H₈₂N₈O₃₁
Molecular Weight:1567.49
Hs Code.:

Synonyms:6'-azido-4',5'-dehydro-3',4'-dideoxy-6,3',2'',5'',3''',4'''-hexa-O-methoxycarbonyl-per-N-Cbz-neomycin

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Chemical Property of 6'-azido-4',5'-dehydro-3',4'-dideoxy-6,3',2'',5'',3''',4'''-hexa-O-methoxycarbonyl-per-N-Cbz-neomycin

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Technology Process of 6'-azido-4',5'-dehydro-3',4'-dideoxy-6,3',2'',5'',3''',4'''-hexa-O-methoxycarbonyl-per-N-Cbz-neomycin

There total 1 articles about 6'-azido-4',5'-dehydro-3',4'-dideoxy-6,3',2'',5'',3''',4'''-hexa-O-methoxycarbonyl-per-N-Cbz-neomycin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1284216-88-1
4',5'-dehydro-3',4'-dideoxy-6,3',2'',5'',3''',4'''-hexa-O-methoxycarbonyl-per-N-Cbz-paromomycin

: 1284216-89-2
6'-azido-4',5'-dehydro-3',4'-dideoxy-6,3',2'',5'',3''',4'''-hexa-O-methoxycarbonyl-per-N-Cbz-neomycin

Guidance literature:: 4',5'-dehydro-3',4'-dideoxy-6,3',2'',5'',3''',4'''-hexa-O-methoxycarbonyl-per-N-Cbz-paromomycin; With diphenyl phosphoryl azide; 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; at 20 - 50 ℃; for 6h;

With water; In tetrahydrofuran;

Reference yield: 70.0%

: 1284216-89-2
6'-azido-4',5'-dehydro-3',4'-dideoxy-6,3',2'',5'',3''',4'''-hexa-O-methoxycarbonyl-per-N-Cbz-neomycin

: 1284216-90-5
6'-azido-4',5'-dehydro-3',4'-dideoxy-per-N-Cbz-neomycin

Guidance literature:: 6'-azido-4',5'-dehydro-3',4'-dideoxy-6,3',2'',5'',3''',4'''-hexa-O-methoxycarbonyl-per-N-Cbz-neomycin; With sodium methylate; In methanol; at 20 ℃; pH=~ 8;

With acetic acid; In methanol;