Technology Process of 6-(p-Tolyl)-dibenzo
cycloheptan
There total 11 articles about 6-(p-Tolyl)-dibenzocycloheptan which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 10 steps
1: (i) Mg, (ii) /BRN= 507387/
2: OsO4, Py
3: CrO3, Py
4: NaBH4
5: (i) aq. NaIO4, (ii) SiO2
6: SiO2 / benzene
7: Ac2O, Py
8: H2 / Pd-C
9: TsOH*H2O / toluene / Heating
10: H2 / Pd-C
With
pyridine; chromium(VI) oxide; sodium tetrahydroborate; osmium(VIII) oxide; hydrogen; acetic anhydride; silica gel; toluene-4-sulfonic acid;
palladium on activated charcoal;
In
toluene; benzene;
DOI:10.1021/jo01034a050
- Guidance literature:
-
Multi-step reaction with 7 steps
1: NaBH4
2: (i) aq. NaIO4, (ii) SiO2
3: SiO2 / benzene
4: Ac2O, Py
5: H2 / Pd-C
6: TsOH*H2O / toluene / Heating
7: H2 / Pd-C
With
pyridine; sodium tetrahydroborate; hydrogen; acetic anhydride; silica gel; toluene-4-sulfonic acid;
palladium on activated charcoal;
In
toluene; benzene;
DOI:10.1021/jo01034a050
- Guidance literature:
-
Multi-step reaction with 8 steps
1: CrO3, Py
2: NaBH4
3: (i) aq. NaIO4, (ii) SiO2
4: SiO2 / benzene
5: Ac2O, Py
6: H2 / Pd-C
7: TsOH*H2O / toluene / Heating
8: H2 / Pd-C
With
pyridine; chromium(VI) oxide; sodium tetrahydroborate; hydrogen; acetic anhydride; silica gel; toluene-4-sulfonic acid;
palladium on activated charcoal;
In
toluene; benzene;
DOI:10.1021/jo01034a050
