ethyl 9-diphenylphosphino-8-nonynoate

Base Information

Chemical Name:ethyl 9-diphenylphosphino-8-nonynoate
CAS No.:935550-34-8
Molecular Formula:C₂₃H₂₇O₂P
Molecular Weight:366.44
Hs Code.:

Synonyms:ethyl 9-diphenylphosphino-8-nonynoate

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Chemical Property of ethyl 9-diphenylphosphino-8-nonynoate

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Technology Process of ethyl 9-diphenylphosphino-8-nonynoate

There total 1 articles about ethyl 9-diphenylphosphino-8-nonynoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 1079-66-9,74391-44-9
chloro-diphenylphosphine

: 108545-40-0
8-nonynoic acid ethyl ester

: 935550-34-8
ethyl 9-diphenylphosphino-8-nonynoate

Guidance literature:: With triethylamine; bis(acetylacetonate)nickel(II); In toluene; at 80 ℃; for 4h;
DOI:10.1021/ja070048d

Reference yield: 77.0%

: 935550-34-8
ethyl 9-diphenylphosphino-8-nonynoate

: 112-55-0
1-dodecylthiol

: ethyl (Z)-9-diphenylphosphino-8-dodecylthio-8-nonenoate

Guidance literature:: palladium diacetate; In ethanol; at 25 ℃; for 1h;
DOI:10.1021/ol0702876

Reference yield:

: 935550-34-8
ethyl 9-diphenylphosphino-8-nonynoate

: ethyl (Z)-8,9-bis(diphenylthiophosphinyl)-8-nonenoate

Guidance literature:: Multi-step reaction with 2 steps

1: CuI; Cs₂CO₃ / dimethylformamide / 4 h / 25 °C

2: S / dimethylformamide / 1 h / 25 °C

With sulfur; copper(l) iodide; caesium carbonate; In N,N-dimethyl-formamide;
DOI:10.1021/ja070048d