N-hydroxy-5-(3-(5-phenylthiophene-2-carboxamido)propyl)-4,5,6,7-tetrahydrothiazolo[5,4-c]pyridine-2-carboxamide

Base Information

• Chemical Name: N-hydroxy-5-(3-(5-phenylthiophene-2-carboxamido)propyl)-4,5,6,7-tetrahydrothiazolo[5,4-c]pyridine-2-carboxamide
• CAS No.: 1391634-40-4
• Molecular Formula: C₂₁H₂₂N₄O₃S₂
• Molecular Weight: 442.563

Synonyms:N-hydroxy-5-(3-(5-phenylthiophene-2-carboxamido)propyl)-4,5,6,7-tetrahydrothiazolo[5,4-c]pyridine-2-carboxamide

Chemical Property of N-hydroxy-5-(3-(5-phenylthiophene-2-carboxamido)propyl)-4,5,6,7-tetrahydrothiazolo[5,4-c]pyridine-2-carboxamide

Chemical Property:

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Technology Process of N-hydroxy-5-(3-(5-phenylthiophene-2-carboxamido)propyl)-4,5,6,7-tetrahydrothiazolo[5,4-c]pyridine-2-carboxamide

There total 2 articles about N-hydroxy-5-(3-(5-phenylthiophene-2-carboxamido)propyl)-4,5,6,7-tetrahydrothiazolo[5,4-c]pyridine-2-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

ethyl 5-(3-(5-phenylthiophene-2-carboxamido)propyl)-4,5,6,7-tetra hydrothiazolo[5,4-c]pyridine-2-carboxylate → N-hydroxy-5-(3-(5-phenylthiophene-2-carboxamido)propyl)-4,5,6,7-tetrahydrothiazolo[5,4-c]pyridine-2-carboxamide (1391634-40-4)

Guidance literature:

With hydroxylamine hydrochloride; potassium hydroxide; In methanol; at 20 ℃; for 0.5h; Inert atmosphere;

DOI:10.1016/j.bmcl.2012.05.123

Reference yield:

C12H20N4O2S → N-hydroxy-5-(3-(5-phenylthiophene-2-carboxamido)propyl)-4,5,6,7-tetrahydrothiazolo[5,4-c]pyridine-2-carboxamide (1391634-40-4)

Guidance literature:

Multi-step reaction with 2 steps

1: triethylamine / dichloromethane / 18 h / 0 - 20 °C / Inert atmosphere

2: hydroxylamine hydrochloride; potassium hydroxide / methanol / 0.5 h / 20 °C / Inert atmosphere

With hydroxylamine hydrochloride; triethylamine; potassium hydroxide; In methanol; dichloromethane;

DOI:10.1016/j.bmcl.2012.05.123

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