ethyl 2-(aminocarbonyl)-3-methoxy-5-methyl-3-phenyl-2H-1,2,3λ⁵-diazaphosphole-4-carboxylate

Base Information

• Chemical Name: ethyl 2-(aminocarbonyl)-3-methoxy-5-methyl-3-phenyl-2H-1,2,3λ⁵-diazaphosphole-4-carboxylate
• CAS No.: 1045710-59-5
• Molecular Formula: C₁₄H₁₈N₃O₄P
• Molecular Weight: 323.288

Synonyms:ethyl 2-(aminocarbonyl)-3-methoxy-5-methyl-3-phenyl-2H-1,2,3λ⁵-diazaphosphole-4-carboxylate

Chemical Property of ethyl 2-(aminocarbonyl)-3-methoxy-5-methyl-3-phenyl-2H-1,2,3λ⁵-diazaphosphole-4-carboxylate

Chemical Property:

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Technology Process of ethyl 2-(aminocarbonyl)-3-methoxy-5-methyl-3-phenyl-2H-1,2,3λ⁵-diazaphosphole-4-carboxylate

There total 2 articles about ethyl 2-(aminocarbonyl)-3-methoxy-5-methyl-3-phenyl-2H-1,2,3λ⁵-diazaphosphole-4-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

phenylphosphonous acid dimethyl ester (2946-61-4) + ethyl 3-[(aminocarbonyl)diazenyl]but-2-enoate (94127-05-6) → ethyl 2-(aminocarbonyl)-3-methoxy-5-methyl-3-phenyl-2H-1,2,3λ5-diazaphosphole-4-carboxylate (1045710-59-5)

Guidance literature:

phenylphosphonous acid dimethyl ester; ethyl 3-[(aminocarbonyl)diazenyl]but-2-enoate; at 20 ℃; for 0.5h;

In tetrahydrofuran; at 20 ℃; for 2h; Further stages.;

DOI:10.1016/j.tet.2008.05.007

Reference yield: 68.0%

ethyl 3-[2-(aminocarbonyl)hydrazono]-2-(1,1-dimethoxy-1-phenyl-λ5-phosphanylidene)butanoate → ethyl 2-(aminocarbonyl)-3-methoxy-5-methyl-3-phenyl-2H-1,2,3λ5-diazaphosphole-4-carboxylate (1045710-59-5)

Guidance literature:

In tetrahydrofuran; at 20 ℃; for 2h;

DOI:10.1016/j.tet.2008.05.007

Reference yield: 81.0%

ethyl 2-(aminocarbonyl)-3-methoxy-5-methyl-3-phenyl-2H-1,2,3λ5-diazaphosphole-4-carboxylate (1045710-59-5) → ethyl (E)-3-[2-(aminocarbonyl)hydrazono]-2-[methoxy(phenyl)phosphoryl]butanoate (1045710-73-3)

Guidance literature:

In methanol; water; at 20 ℃; for 10h;

DOI:10.1016/j.tet.2008.05.007

upstream raw materials:

phenylphosphonous acid dimethyl ester

ethyl 3-[(aminocarbonyl)diazenyl]but-2-enoate

Downstream raw materials:

ethyl (E)-3-[2-(aminocarbonyl)hydrazono]-2-[methoxy(phenyl)phosphoryl]butanoate

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