N-[(1,4-dichloro-7-isoquinolinyl)sulphonyl]-N-(3-chlorobenzyl)glycine t-butyl ester

Base Information

Chemical Name:N-[(1,4-dichloro-7-isoquinolinyl)sulphonyl]-N-(3-chlorobenzyl)glycine t-butyl ester
CAS No.:256477-41-5
Molecular Formula:C₂₂H₂₁Cl₃N₂O₄S
Molecular Weight:515.845
Hs Code.:

Synonyms:N-[(1,4-dichloro-7-isoquinolinyl)sulphonyl]-N-(3-chlorobenzyl)glycine t-butyl ester

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Chemical Property of N-[(1,4-dichloro-7-isoquinolinyl)sulphonyl]-N-(3-chlorobenzyl)glycine t-butyl ester

Chemical Property:

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Technology Process of N-[(1,4-dichloro-7-isoquinolinyl)sulphonyl]-N-(3-chlorobenzyl)glycine t-butyl ester

There total 4 articles about N-[(1,4-dichloro-7-isoquinolinyl)sulphonyl]-N-(3-chlorobenzyl)glycine t-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 256477-27-7
N-[(1,4-dichloro-7-isoquinolinyl)sulphonyl]glycine tert-butyl ester

: 620-20-2,130468-19-8
1-Chloro-3-chloromethyl-benzene

: 256477-41-5
N-[(1,4-dichloro-7-isoquinolinyl)sulphonyl]-N-(3-chlorobenzyl)glycine t-butyl ester

Guidance literature:: In potassium carbonate; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 223671-80-5
1,4-dichloro-7-isoquinolinesulphonyl chloride

: 256477-41-5
N-[(1,4-dichloro-7-isoquinolinyl)sulphonyl]-N-(3-chlorobenzyl)glycine t-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / dichloromethane

2: potassium carbonate; ethyl acetate; N,N-dimethyl-formamide

With triethylamine; In dichloromethane; potassium carbonate; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 223671-81-6
4-chloro-1-oxo-1,2-dihydro-7-isoquinolinesulfonyl chloride

: 256477-41-5
N-[(1,4-dichloro-7-isoquinolinyl)sulphonyl]-N-(3-chlorobenzyl)glycine t-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: trichlorophosphate / diethyl ether; acetonitrile

2: triethylamine / dichloromethane

3: potassium carbonate; ethyl acetate; N,N-dimethyl-formamide

With triethylamine; trichlorophosphate; In diethyl ether; dichloromethane; potassium carbonate; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;