splenocin B

Base Information

Chemical Name:splenocin B
CAS No.:1148106-17-5
Molecular Formula:C₂₈H₃₂N₂O₉
Molecular Weight:540.57
Hs Code.:

Synonyms:splenocin B

Suppliers and Price of splenocin B

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of splenocin B

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of splenocin B

There total 8 articles about splenocin B which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: C₃₅H₃₈N₂O₉

: 1148106-17-5
splenocin B

Guidance literature:: With 4-methyl-morpholine; In ethanol; at 20 ℃; for 15h; under 760.051 Torr;
DOI:10.1016/j.tet.2015.10.075

Reference yield:

: 210300-08-6
(2R,3R,4S)-2-benzyl-3-(tert-butyldimethylsilanyloxy)-4-hydroxypentanoic acid benzyl ester

: 1148106-17-5
splenocin B

Guidance literature:: Multi-step reaction with 9 steps

1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 0 - 20 °C

2: hydrogen / ethanol / 20 °C / 760.05 Torr

3: [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂ / hexane; acetone / 1 h / 0 - 20 °C / Inert atmosphere

4: 10-camphorsufonic acid / dichloromethane; acetonitrile / 24 h / 80 °C

5: pyridine hydrogenfluoride; pyridine / tetrahydrofuran / 20 °C

6: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

7: trifluoroacetic acid / 2 h / 20 °C

8: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; 4-methyl-morpholine / N,N-dimethyl-formamide / 18 h / 20 °C

9: 4-methyl-morpholine / ethanol / 15 h / 20 °C / 760.05 Torr

With 4-methyl-morpholine; pyridine; dmap; [ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂; 10-camphorsufonic acid; hydrogen; benzotriazol-1-ol; pyridine hydrogenfluoride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In tetrahydrofuran; ethanol; hexane; dichloromethane; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1016/j.tet.2015.10.075

Reference yield:

: C₃₁H₅₁NO₉Si

: 1148106-17-5
splenocin B

Guidance literature:: Multi-step reaction with 6 steps

1: 10-camphorsufonic acid / dichloromethane; acetonitrile / 24 h / 80 °C

2: pyridine hydrogenfluoride; pyridine / tetrahydrofuran / 20 °C

3: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 20 °C

4: trifluoroacetic acid / 2 h / 20 °C

5: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; 4-methyl-morpholine / N,N-dimethyl-formamide / 18 h / 20 °C

6: 4-methyl-morpholine / ethanol / 15 h / 20 °C / 760.05 Torr

With 4-methyl-morpholine; pyridine; dmap; 10-camphorsufonic acid; benzotriazol-1-ol; pyridine hydrogenfluoride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; trifluoroacetic acid; In tetrahydrofuran; ethanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.tet.2015.10.075