3-[(S)-3-Oxo-3-[4-(piperazine-1-carbonyl)-piperidin-1-yl]-2-(2,4,6-triisopropyl-benzenesulfonylamino)-propyl]-benzamidine

Base Information

Chemical Name:3-[(S)-3-Oxo-3-[4-(piperazine-1-carbonyl)-piperidin-1-yl]-2-(2,4,6-triisopropyl-benzenesulfonylamino)-propyl]-benzamidine
CAS No.:797040-69-8
Molecular Formula:C₃₅H₅₂N₆O₄S
Molecular Weight:652.902
Hs Code.:

Synonyms:3-[(S)-3-Oxo-3-[4-(piperazine-1-carbonyl)-piperidin-1-yl]-2-(2,4,6-triisopropyl-benzenesulfonylamino)-propyl]-benzamidine

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Chemical Property of 3-[(S)-3-Oxo-3-[4-(piperazine-1-carbonyl)-piperidin-1-yl]-2-(2,4,6-triisopropyl-benzenesulfonylamino)-propyl]-benzamidine

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Technology Process of 3-[(S)-3-Oxo-3-[4-(piperazine-1-carbonyl)-piperidin-1-yl]-2-(2,4,6-triisopropyl-benzenesulfonylamino)-propyl]-benzamidine

There total 5 articles about 3-[(S)-3-Oxo-3-[4-(piperazine-1-carbonyl)-piperidin-1-yl]-2-(2,4,6-triisopropyl-benzenesulfonylamino)-propyl]-benzamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₇H₅₄N₆O₆S

: 797040-69-8
3-[(S)-3-Oxo-3-[4-(piperazine-1-carbonyl)-piperidin-1-yl]-2-(2,4,6-triisopropyl-benzenesulfonylamino)-propyl]-benzamidine

Guidance literature:: With hydrogen; acetic acid; palladium on activated charcoal; at 40 ℃;
DOI:10.1021/jm051272l

Reference yield:

: 255374-80-2
Nα-2,4,6-Triisopropylphenylsulfonyl-(L)-3-cyano-phenylalanine

: 797040-69-8
3-[(S)-3-Oxo-3-[4-(piperazine-1-carbonyl)-piperidin-1-yl]-2-(2,4,6-triisopropyl-benzenesulfonylamino)-propyl]-benzamidine

Guidance literature:: Multi-step reaction with 5 steps

1: hydroxylamine*HCl; diisopropylethylamine / ethanol / Heating

2: AcOH / 20 °C

3: PyBop; diisopropylethylamine / dimethylformamide / 0 - 20 °C

4: aq. HCl; AcOH / 20 °C

5: aq. AcOH; H₂ / Pd/C / 40 °C

With hydrogenchloride; hydroxylamine hydrochloride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; acetic acid; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm051272l

Reference yield:

: 797040-06-3
C₂₇H₃₇N₃O₆S

: 797040-69-8
3-[(S)-3-Oxo-3-[4-(piperazine-1-carbonyl)-piperidin-1-yl]-2-(2,4,6-triisopropyl-benzenesulfonylamino)-propyl]-benzamidine

Guidance literature:: Multi-step reaction with 3 steps

1: PyBop; diisopropylethylamine / dimethylformamide / 0 - 20 °C

2: aq. HCl; AcOH / 20 °C

3: aq. AcOH; H₂ / Pd/C / 40 °C

With hydrogenchloride; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; hydrogen; acetic acid; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In N,N-dimethyl-formamide;
DOI:10.1021/jm051272l