C₃₄H₅₉NO₄Si₂

Base Information

Chemical Name:C₃₄H₅₉NO₄Si₂
CAS No.:1351993-14-0
Molecular Formula:C₃₄H₅₉NO₄Si₂
Molecular Weight:602.018
Hs Code.:

C<sub>34</sub>H<sub>59</sub>NO<sub>4</sub>Si<sub>2</sub>

Synonyms:C₃₄H₅₉NO₄Si₂

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Chemical Property of C₃₄H₅₉NO₄Si₂

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Technology Process of C₃₄H₅₉NO₄Si₂

There total 12 articles about C₃₄H₅₉NO₄Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₄H₅₇NO₄Si₂

: 1351993-14-0
C₃₄H₅₉NO₄Si₂

Guidance literature:: With sodium tetrahydroborate; In methanol; dimethyl sulfoxide; at 0 ℃; for 0.166667h; Inert atmosphere;
DOI:10.1016/j.tetasy.2011.09.017

Reference yield:

: 1351993-02-6
(S)-methyl 4-hydroxy-8-phenyloctanoate

: 1351993-14-0
C₃₄H₅₉NO₄Si₂

Guidance literature:: Multi-step reaction with 9 steps

1: 1H-imidazole / dichloromethane / 0 - 20 °C / Inert atmosphere

2: diisobutylaluminium hydride / dichloromethane / -78 °C / Inert atmosphere

3: D-Prolin / dimethyl sulfoxide / 1 h / 25 °C / Inert atmosphere

4: 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride / dimethyl sulfoxide / 1 h / 0 - 20 °C / Inert atmosphere

5: palladium 10% on activated carbon; hydrogen / ethyl acetate / 8 h

6: 1H-imidazole / dichloromethane / 0 - 20 °C / Inert atmosphere

7: diisobutylaluminium hydride / dichloromethane; toluene / 1 h / 0 - 20 °C / Inert atmosphere

8: D-Prolin / dimethyl sulfoxide / 1 h / 25 °C / Inert atmosphere

9: sodium tetrahydroborate / methanol; dimethyl sulfoxide / 0.17 h / 0 °C / Inert atmosphere

With 1H-imidazole; sodium tetrahydroborate; palladium 10% on activated carbon; hydrogen; diisobutylaluminium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; D-Prolin; lithium chloride; In methanol; dichloromethane; dimethyl sulfoxide; ethyl acetate; toluene; 4: Horner-Wadsworth-Emmons olefination;
DOI:10.1016/j.tetasy.2011.09.017

Reference yield:

: 1351993-03-7
(S)-methyl 4-(tert-butyldimethylsilyloxy)-8-phenyloctanoate

: 1351993-14-0
C₃₄H₅₉NO₄Si₂

Guidance literature:: Multi-step reaction with 8 steps

1: diisobutylaluminium hydride / dichloromethane / -78 °C / Inert atmosphere

2: D-Prolin / dimethyl sulfoxide / 1 h / 25 °C / Inert atmosphere

3: 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride / dimethyl sulfoxide / 1 h / 0 - 20 °C / Inert atmosphere

4: palladium 10% on activated carbon; hydrogen / ethyl acetate / 8 h

5: 1H-imidazole / dichloromethane / 0 - 20 °C / Inert atmosphere

6: diisobutylaluminium hydride / dichloromethane; toluene / 1 h / 0 - 20 °C / Inert atmosphere

7: D-Prolin / dimethyl sulfoxide / 1 h / 25 °C / Inert atmosphere

8: sodium tetrahydroborate / methanol; dimethyl sulfoxide / 0.17 h / 0 °C / Inert atmosphere

With 1H-imidazole; sodium tetrahydroborate; palladium 10% on activated carbon; hydrogen; diisobutylaluminium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; D-Prolin; lithium chloride; In methanol; dichloromethane; dimethyl sulfoxide; ethyl acetate; toluene; 3: Horner-Wadsworth-Emmons olefination;
DOI:10.1016/j.tetasy.2011.09.017