C₂₆H₃₂O₆

Base Information

Chemical Name:C₂₆H₃₂O₆
CAS No.:942068-63-5
Molecular Formula:C₂₆H₃₂O₆
Molecular Weight:440.536
Hs Code.:

C<sub>26</sub>H<sub>32</sub>O<sub>6</sub>

Synonyms:C₂₆H₃₂O₆

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Chemical Property of C₂₆H₃₂O₆

Chemical Property:

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Technology Process of C₂₆H₃₂O₆

There total 13 articles about C₂₆H₃₂O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₃H₂₈O₄

: 942068-63-5
C₂₆H₃₂O₆

Guidance literature:: Multi-step reaction with 11 steps

1.1: 58 percent / Cl₂[(c-C₆H₁₁)3P](1,3-dimesitylimidazolidin-2-ylidene)Ru=CHPh / toluene / 20 - 70 °C

2.1: CH₂Cl₂; acetone / 1 h / 0 °C

3.1: BF₃*OEt₂; triethylsilane / acetonitrile / -40 - 20 °C

4.1: 77 percent / triethylamine; 4-(dimethylamino)pyridine / CH₂Cl₂

5.1: sodium hydride; tetrabutylammonium iodide / tetrahydrofuran / 6 h / Heating

6.1: 410 mg / diethyl ether; H₂O / 1 h / 20 °C

7.1: 70 percent / Cl₂[(c-C₆H₁₁)3P](1,3-dimesitylimidazolidin-2-ylidene)Ru=CHPh / CH₂Cl₂ / Heating

8.1: Mg₂SO₄; acetic acid / benzene / 0.83 h / 20 °C

9.1: t-BuLi / tetrahydrofuran; pentane / 0.08 h / -78 °C

9.2: tetrahydrofuran; pentane / 0.33 h / -78 - 20 °C

10.1: 89.4 mg / CuCl₂ / tetrahydrofuran; H₂O / 1 h / 20 °C

11.1: cerium(III) chloride heptahydrate; sodium borohydride / methanol / 1 h / -78 °C

With triethylsilane; dmap; sodium tetrahydroborate; cerium(III) chloride; boron trifluoride diethyl etherate; tert.-butyl lithium; tetra-(n-butyl)ammonium iodide; sodium hydride; magnesium sulfate; acetic acid; triethylamine; copper dichloride; Cl₂[(c-C₆H₁₁)3P](1,3-dimesitylimidazolidin-2-ylidene)Ru=CHPh; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; acetone; toluene; acetonitrile; pentane; benzene;
DOI:10.1021/ol0706096

Reference yield:

: 942068-54-4
C₂₁H₂₄O₄

: 942068-63-5
C₂₆H₃₂O₆

Guidance literature:: Multi-step reaction with 10 steps

1.1: CH₂Cl₂; acetone / 1 h / 0 °C

2.1: BF₃*OEt₂; triethylsilane / acetonitrile / -40 - 20 °C

3.1: 77 percent / triethylamine; 4-(dimethylamino)pyridine / CH₂Cl₂

4.1: sodium hydride; tetrabutylammonium iodide / tetrahydrofuran / 6 h / Heating

5.1: 410 mg / diethyl ether; H₂O / 1 h / 20 °C

6.1: 70 percent / Cl₂[(c-C₆H₁₁)3P](1,3-dimesitylimidazolidin-2-ylidene)Ru=CHPh / CH₂Cl₂ / Heating

7.1: Mg₂SO₄; acetic acid / benzene / 0.83 h / 20 °C

8.1: t-BuLi / tetrahydrofuran; pentane / 0.08 h / -78 °C

8.2: tetrahydrofuran; pentane / 0.33 h / -78 - 20 °C

9.1: 89.4 mg / CuCl₂ / tetrahydrofuran; H₂O / 1 h / 20 °C

10.1: cerium(III) chloride heptahydrate; sodium borohydride / methanol / 1 h / -78 °C

With triethylsilane; dmap; sodium tetrahydroborate; cerium(III) chloride; boron trifluoride diethyl etherate; tert.-butyl lithium; tetra-(n-butyl)ammonium iodide; sodium hydride; magnesium sulfate; acetic acid; triethylamine; copper dichloride; Cl₂[(c-C₆H₁₁)3P](1,3-dimesitylimidazolidin-2-ylidene)Ru=CHPh; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; acetone; acetonitrile; pentane; benzene;
DOI:10.1021/ol0706096

Reference yield:

: C₂₁H₂₄O₅

: 942068-63-5
C₂₆H₃₂O₆

Guidance literature:: Multi-step reaction with 9 steps

1.1: BF₃*OEt₂; triethylsilane / acetonitrile / -40 - 20 °C

2.1: 77 percent / triethylamine; 4-(dimethylamino)pyridine / CH₂Cl₂

3.1: sodium hydride; tetrabutylammonium iodide / tetrahydrofuran / 6 h / Heating

4.1: 410 mg / diethyl ether; H₂O / 1 h / 20 °C

5.1: 70 percent / Cl₂[(c-C₆H₁₁)3P](1,3-dimesitylimidazolidin-2-ylidene)Ru=CHPh / CH₂Cl₂ / Heating

6.1: Mg₂SO₄; acetic acid / benzene / 0.83 h / 20 °C

7.1: t-BuLi / tetrahydrofuran; pentane / 0.08 h / -78 °C

7.2: tetrahydrofuran; pentane / 0.33 h / -78 - 20 °C

8.1: 89.4 mg / CuCl₂ / tetrahydrofuran; H₂O / 1 h / 20 °C

9.1: cerium(III) chloride heptahydrate; sodium borohydride / methanol / 1 h / -78 °C

With triethylsilane; dmap; sodium tetrahydroborate; cerium(III) chloride; boron trifluoride diethyl etherate; tert.-butyl lithium; tetra-(n-butyl)ammonium iodide; sodium hydride; magnesium sulfate; acetic acid; triethylamine; copper dichloride; Cl₂[(c-C₆H₁₁)3P](1,3-dimesitylimidazolidin-2-ylidene)Ru=CHPh; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; acetonitrile; pentane; benzene;
DOI:10.1021/ol0706096