ethyl 3a-[2-(aminocarbonyl)hydrazino]-2-(4-chlorophenyl)-3a,4,5,6,7,7a-hexahydro-1,3-benzothiazole-7a-carboxylate

Base Information

Chemical Name:ethyl 3a-[2-(aminocarbonyl)hydrazino]-2-(4-chlorophenyl)-3a,4,5,6,7,7a-hexahydro-1,3-benzothiazole-7a-carboxylate
CAS No.:936088-29-8
Molecular Formula:C₁₇H₂₁ClN₄O₃S
Molecular Weight:396.898
Hs Code.:

Synonyms:ethyl 3a-[2-(aminocarbonyl)hydrazino]-2-(4-chlorophenyl)-3a,4,5,6,7,7a-hexahydro-1,3-benzothiazole-7a-carboxylate

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Chemical Property of ethyl 3a-[2-(aminocarbonyl)hydrazino]-2-(4-chlorophenyl)-3a,4,5,6,7,7a-hexahydro-1,3-benzothiazole-7a-carboxylate

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Technology Process of ethyl 3a-[2-(aminocarbonyl)hydrazino]-2-(4-chlorophenyl)-3a,4,5,6,7,7a-hexahydro-1,3-benzothiazole-7a-carboxylate

There total 1 articles about ethyl 3a-[2-(aminocarbonyl)hydrazino]-2-(4-chlorophenyl)-3a,4,5,6,7,7a-hexahydro-1,3-benzothiazole-7a-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: ethyl 2-[2-(aminocarbonyl)-1-diazenyl]-1-cyclohexene-1-carboxylate

: 2521-24-6
4-chlorothiobenzamide

: 936088-29-8
ethyl 3a-[2-(aminocarbonyl)hydrazino]-2-(4-chlorophenyl)-3a,4,5,6,7,7a-hexahydro-1,3-benzothiazole-7a-carboxylate

Guidance literature:: In methanol; at 20 ℃;
DOI:10.1016/j.tetlet.2007.02.041 DOI:10.1016/j.tet.2008.01.102

Reference yield: 67.0%

: 936088-29-8
ethyl 3a-[2-(aminocarbonyl)hydrazino]-2-(4-chlorophenyl)-3a,4,5,6,7,7a-hexahydro-1,3-benzothiazole-7a-carboxylate

: 1025066-49-2
ethyl 1-[(4-chlorobenzoyl)thio]-2-oxocyclohexane-1-carboxylate

: 1025066-46-9
ethyl 1-[(4-chlorobenzoyl)thio]-2-iminocyclohexane-1-carboxylate

Guidance literature:: With Amberlyst 15H; In water; acetone; at 20 ℃;
DOI:10.1016/j.tet.2008.01.102

Reference yield: 59.0%

: 936088-29-8
ethyl 3a-[2-(aminocarbonyl)hydrazino]-2-(4-chlorophenyl)-3a,4,5,6,7,7a-hexahydro-1,3-benzothiazole-7a-carboxylate

: 11-(4-chlorophenyl)-10-thia-7,8,12-triazatricyclo[4.3.3.0^1,6]dodec-11-en-9-one

Guidance literature:: ethyl 3a-[2-(aminocarbonyl)hydrazino]-2-(4-chlorophenyl)-3a,4,5,6,7,7a-hexahydro-1,3-benzothiazole-7a-carboxylate; With sodium hydride; In tetrahydrofuran; at 20 ℃;

With Amberlyst 15H; In tetrahydrofuran; at 20 ℃; for 0.166667h;
DOI:10.1016/j.tetlet.2007.02.041