2-chloro-4-(((6-cyanobiphenyl-3-yl)(4H-1,2,4-triazol-4-yl)amino)methyl)-phenyl sulfamate

Base Information

Chemical Name:2-chloro-4-(((6-cyanobiphenyl-3-yl)(4H-1,2,4-triazol-4-yl)amino)methyl)-phenyl sulfamate
CAS No.:1260389-38-5
Molecular Formula:C₂₂H₁₇ClN₆O₃S
Molecular Weight:480.934
Hs Code.:

Synonyms:2-chloro-4-(((6-cyanobiphenyl-3-yl)(4H-1,2,4-triazol-4-yl)amino)methyl)-phenyl sulfamate

Suppliers and Price of 2-chloro-4-(((6-cyanobiphenyl-3-yl)(4H-1,2,4-triazol-4-yl)amino)methyl)-phenyl sulfamate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-chloro-4-(((6-cyanobiphenyl-3-yl)(4H-1,2,4-triazol-4-yl)amino)methyl)-phenyl sulfamate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-chloro-4-(((6-cyanobiphenyl-3-yl)(4H-1,2,4-triazol-4-yl)amino)methyl)-phenyl sulfamate

There total 8 articles about 2-chloro-4-(((6-cyanobiphenyl-3-yl)(4H-1,2,4-triazol-4-yl)amino)methyl)-phenyl sulfamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 1260389-56-7
5-((3-chloro-4-hydroxybenzyl)(4H-1,2,4-triazol-4-yl)amino)biphenyl-2-carbonitrile

: 1260389-38-5
2-chloro-4-(((6-cyanobiphenyl-3-yl)(4H-1,2,4-triazol-4-yl)amino)methyl)-phenyl sulfamate

Guidance literature:: With sulphamoyl chloride; In N,N-dimethyl acetamide; at 0 - 20 ℃; for 6h;

Reference yield:

: 36282-26-5
2-bromo-4-fluorobenzonitrile

: 1260389-38-5
2-chloro-4-(((6-cyanobiphenyl-3-yl)(4H-1,2,4-triazol-4-yl)amino)methyl)-phenyl sulfamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium carbonate / bis(dibenzylideneacetone)-palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 5 h / Heating; Reflux; Inert atmosphere

2.1: potassium tert-butylate / dimethyl sulfoxide / 0.5 h / 20 °C

2.2: 1 h / 20 °C

3.1: potassium carbonate / N,N-dimethyl-formamide

4.1: sulphamoyl chloride / N,N-dimethyl acetamide / 6 h / 0 - 20 °C

With sulphamoyl chloride; potassium tert-butylate; sodium carbonate; potassium carbonate; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In 1,2-dimethoxyethane; N,N-dimethyl acetamide; water; dimethyl sulfoxide; N,N-dimethyl-formamide;

Reference yield:

: 98-80-6
phenylboronic acid

: 1260389-38-5
2-chloro-4-(((6-cyanobiphenyl-3-yl)(4H-1,2,4-triazol-4-yl)amino)methyl)-phenyl sulfamate

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium carbonate / bis(dibenzylideneacetone)-palladium⁽⁰⁾ / 1,2-dimethoxyethane; water / 5 h / Heating; Reflux; Inert atmosphere

2.1: potassium tert-butylate / dimethyl sulfoxide / 0.5 h / 20 °C

2.2: 1 h / 20 °C

3.1: potassium carbonate / N,N-dimethyl-formamide

4.1: sulphamoyl chloride / N,N-dimethyl acetamide / 6 h / 0 - 20 °C

With sulphamoyl chloride; potassium tert-butylate; sodium carbonate; potassium carbonate; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In 1,2-dimethoxyethane; N,N-dimethyl acetamide; water; dimethyl sulfoxide; N,N-dimethyl-formamide;