(2R,3S,4S,5S,6R)-2-Hydroxymethyl-6-(4-octyloxy-phenylsulfanyl)-tetrahydro-pyran-3,4,5-triol

Base Information

Chemical Name:(2R,3S,4S,5S,6R)-2-Hydroxymethyl-6-(4-octyloxy-phenylsulfanyl)-tetrahydro-pyran-3,4,5-triol
CAS No.:916497-86-4
Molecular Formula:C₂₀H₃₂O₆S
Molecular Weight:400.536
Hs Code.:

Synonyms:(2R,3S,4S,5S,6R)-2-Hydroxymethyl-6-(4-octyloxy-phenylsulfanyl)-tetrahydro-pyran-3,4,5-triol

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Chemical Property of (2R,3S,4S,5S,6R)-2-Hydroxymethyl-6-(4-octyloxy-phenylsulfanyl)-tetrahydro-pyran-3,4,5-triol

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Technology Process of (2R,3S,4S,5S,6R)-2-Hydroxymethyl-6-(4-octyloxy-phenylsulfanyl)-tetrahydro-pyran-3,4,5-triol

There total 3 articles about (2R,3S,4S,5S,6R)-2-Hydroxymethyl-6-(4-octyloxy-phenylsulfanyl)-tetrahydro-pyran-3,4,5-triol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 916497-79-5
Acetic acid (2R,3S,4S,5R,6R)-4,5-diacetoxy-6-acetoxymethyl-2-(4-octyloxy-phenylsulfanyl)-tetrahydro-pyran-3-yl ester

: 916497-86-4
(2R,3S,4S,5S,6R)-2-Hydroxymethyl-6-(4-octyloxy-phenylsulfanyl)-tetrahydro-pyran-3,4,5-triol

Guidance literature:: With potassium hydroxide; In methanol;
DOI:10.1016/j.bmcl.2006.08.095

Reference yield:

: 21095-40-9
4-(octyloxy)benzene-1-sulfonyl chloride

: 916497-86-4
(2R,3S,4S,5S,6R)-2-Hydroxymethyl-6-(4-octyloxy-phenylsulfanyl)-tetrahydro-pyran-3,4,5-triol

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminum hydride / tetrahydrofuran / 10 h / Heating

2: 96 percent / boron trifluoride diethyl etherate / CH₂Cl₂ / 12 h / 20 °C

3: 100 percent / potassium hydroxide / methanol

With potassium hydroxide; lithium aluminium tetrahydride; boron trifluoride diethyl etherate; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.bmcl.2006.08.095

Reference yield:

: Sodium; 4-octyloxy-benzenesulfonate

: 916497-86-4
(2R,3S,4S,5S,6R)-2-Hydroxymethyl-6-(4-octyloxy-phenylsulfanyl)-tetrahydro-pyran-3,4,5-triol

Guidance literature:: Multi-step reaction with 4 steps

1: thionyl chloride / Heating

2: lithium aluminum hydride / tetrahydrofuran / 10 h / Heating

3: 96 percent / boron trifluoride diethyl etherate / CH₂Cl₂ / 12 h / 20 °C

4: 100 percent / potassium hydroxide / methanol

With potassium hydroxide; lithium aluminium tetrahydride; thionyl chloride; boron trifluoride diethyl etherate; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1016/j.bmcl.2006.08.095