9-benzyl-2-tert-but yl-7-isopropyl-3-phenyl-1-oxa-2,7,9-triazaspiro[4.5]decane-6,8-dione

Base Information

Chemical Name:9-benzyl-2-tert-but yl-7-isopropyl-3-phenyl-1-oxa-2,7,9-triazaspiro[4.5]decane-6,8-dione
CAS No.:1586023-66-6
Molecular Formula:C₂₆H₃₃N₃O₃
Molecular Weight:435.566
Hs Code.:

Synonyms:9-benzyl-2-tert-but yl-7-isopropyl-3-phenyl-1-oxa-2,7,9-triazaspiro[4.5]decane-6,8-dione

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Chemical Property of 9-benzyl-2-tert-but yl-7-isopropyl-3-phenyl-1-oxa-2,7,9-triazaspiro[4.5]decane-6,8-dione

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Technology Process of 9-benzyl-2-tert-but yl-7-isopropyl-3-phenyl-1-oxa-2,7,9-triazaspiro[4.5]decane-6,8-dione

There total 3 articles about 9-benzyl-2-tert-but yl-7-isopropyl-3-phenyl-1-oxa-2,7,9-triazaspiro[4.5]decane-6,8-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 1586023-56-4
ethyl 5-{[benzyl(N-isopropylcarbamoyl)amino]methyl}-2-tert-butyl-3-phenylisoxazolidine-5-carboxylate

: 1586023-66-6
9-benzyl-2-tert-but yl-7-isopropyl-3-phenyl-1-oxa-2,7,9-triazaspiro[4.5]decane-6,8-dione

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; for 1h;
DOI:10.3184/174751913X13783169779948

Reference yield:

: 256498-22-3
C₁₃H₁₇NO₂

: 1586023-66-6
9-benzyl-2-tert-but yl-7-isopropyl-3-phenyl-1-oxa-2,7,9-triazaspiro[4.5]decane-6,8-dione

Guidance literature:: Multi-step reaction with 3 steps

1: toluene / Inert atmosphere; Reflux

2: toluene / 24 h / 80 °C / Inert atmosphere

3: potassium tert-butylate / tetrahydrofuran / 1 h

With potassium tert-butylate; In tetrahydrofuran; toluene;
DOI:10.3184/174751913X13783169779948

Reference yield:

: 100-46-9
benzylamine

: 1586023-66-6
9-benzyl-2-tert-but yl-7-isopropyl-3-phenyl-1-oxa-2,7,9-triazaspiro[4.5]decane-6,8-dione

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / chloroform

2: toluene / Inert atmosphere; Reflux

3: toluene / 24 h / 80 °C / Inert atmosphere

4: potassium tert-butylate / tetrahydrofuran / 1 h

With potassium tert-butylate; triethylamine; In tetrahydrofuran; chloroform; toluene;
DOI:10.3184/174751913X13783169779948