13-benzyl hydrogen 12,13-secototara-8⁽¹⁴⁾,9⁽¹¹⁾-diene-12,13-dioate

Base Information

Chemical Name:13-benzyl hydrogen 12,13-secototara-8⁽¹⁴⁾,9⁽¹¹⁾-diene-12,13-dioate
CAS No.:142791-45-5
Molecular Formula:C₂₇H₃₆O₄
Molecular Weight:424.58
Hs Code.:

13-benzyl hydrogen 12,13-secototara-8<sup>(14)</sup>,9<sup>(11)</sup>-diene-12,13-dioate

Synonyms:13-benzyl hydrogen 12,13-secototara-8⁽¹⁴⁾,9⁽¹¹⁾-diene-12,13-dioate

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Chemical Property of 13-benzyl hydrogen 12,13-secototara-8⁽¹⁴⁾,9⁽¹¹⁾-diene-12,13-dioate

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Technology Process of 13-benzyl hydrogen 12,13-secototara-8⁽¹⁴⁾,9⁽¹¹⁾-diene-12,13-dioate

There total 8 articles about 13-benzyl hydrogen 12,13-secototara-8⁽¹⁴⁾,9⁽¹¹⁾-diene-12,13-dioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 142791-44-4
13-benzyl 12-methyl 12,13-secototara-8⁽¹⁴⁾,9⁽¹¹⁾-diene-12,13-dioate

: 142791-45-5
13-benzyl hydrogen 12,13-secototara-8⁽¹⁴⁾,9⁽¹¹⁾-diene-12,13-dioate

Guidance literature:: With potassium hydroxide; In methanol; for 5h; Heating;

Reference yield: 26.0%

: 142791-35-3
13-benzyloxytotara-8,11,13-trien-12-ol

: 142791-45-5
13-benzyl hydrogen 12,13-secototara-8⁽¹⁴⁾,9⁽¹¹⁾-diene-12,13-dioate

Guidance literature:: With ozone; In methanol; dichloromethane; at -78 ℃;

Reference yield:

: 1212475-14-3
Totarol

: 142791-45-5
13-benzyl hydrogen 12,13-secototara-8⁽¹⁴⁾,9⁽¹¹⁾-diene-12,13-dioate

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) NaOH / 1.) EtOH, reflux, 1 h, 2.) EtOH, RT, 90 h

2: 64 percent / Br₂, K₂CO₃, AcOTl / CCl₄ / 1 h / Ambient temperature

3: 1.) BuLi, 2.) O₂ / 1.) Et₂O, hexane, 0 deg C, 90 s, 2.) Et₂O, hexane, 25 min

4: 1.) KOH / 1.) EtOH, reflux, 2 h, 2.) EtOH, RT, 18 h

5: 100 percent / O₃ / CH₂Cl₂; methanol / -78 °C

6: 71 percent / aq. KOH / methanol / 5 h / Heating

With potassium hydroxide; sodium hydroxide; n-butyllithium; bromine; oxygen; thallium(I) acetate; potassium carbonate; ozone; In methanol; tetrachloromethane; dichloromethane;