2-(5-((2-ethylhexyl)carbamoyl)-2,4-bis((2-ethylhexyl)oxy)benzamido)acetic acid

Base Information

Chemical Name:2-(5-((2-ethylhexyl)carbamoyl)-2,4-bis((2-ethylhexyl)oxy)benzamido)acetic acid
CAS No.:1260632-44-7
Molecular Formula:C₃₄H₅₈N₂O₆
Molecular Weight:590.844
Hs Code.:

Synonyms:2-(5-((2-ethylhexyl)carbamoyl)-2,4-bis((2-ethylhexyl)oxy)benzamido)acetic acid

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Chemical Property of 2-(5-((2-ethylhexyl)carbamoyl)-2,4-bis((2-ethylhexyl)oxy)benzamido)acetic acid

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Technology Process of 2-(5-((2-ethylhexyl)carbamoyl)-2,4-bis((2-ethylhexyl)oxy)benzamido)acetic acid

There total 2 articles about 2-(5-((2-ethylhexyl)carbamoyl)-2,4-bis((2-ethylhexyl)oxy)benzamido)acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: C₃₆H₆₂N₂O₆

: 1260632-44-7
2-(5-((2-ethylhexyl)carbamoyl)-2,4-bis((2-ethylhexyl)oxy)benzamido)acetic acid

Guidance literature:: With water; sodium hydroxide; In methanol; for 6h;
DOI:10.1021/ol102522m

Reference yield:

: 1260632-42-5
5-((2-ethylhexyl)carbamoyl)-2,4-bis((2-ethylhexyl)oxy)benzoic acid

: 1260632-44-7
2-(5-((2-ethylhexyl)carbamoyl)-2,4-bis((2-ethylhexyl)oxy)benzamido)acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride / dichloromethane / 2 h / Inert atmosphere

1.2: 24 h / Inert atmosphere

2.1: water; sodium hydroxide / methanol / 6 h

With water; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; sodium hydroxide; In methanol; dichloromethane;
DOI:10.1021/ol102522m

Reference yield: 86.0%

: 1260632-44-7
2-(5-((2-ethylhexyl)carbamoyl)-2,4-bis((2-ethylhexyl)oxy)benzamido)acetic acid

: 613-76-3
2,7-diaminonaphthalene

: 1260632-55-0
N⁽¹⁾,N⁽¹⁾'-((naphthalene-2,7-diylbis(azanediyl))bis(2-oxoethane-2,1-diyl))bis(N⁽³⁾-(2-ethylhexyl)-4,6-bis((2-ethylhexyl)oxy)isophthalamide)

Guidance literature:: 2-(5-((2-ethylhexyl)carbamoyl)-2,4-bis((2-ethylhexyl)oxy)benzamido)acetic acid; With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In dichloromethane; for 2h; Inert atmosphere;

2,7-diaminonaphthalene; In dichloromethane; at 20 ℃; for 30h; Inert atmosphere; Reflux;
DOI:10.1021/ol102522m