6-{2-[allyloxycarbonyl-(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-amino]-acetylamino}-hexanoic acid tert-butyl ester

Base Information

Chemical Name:6-{2-[allyloxycarbonyl-(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-amino]-acetylamino}-hexanoic acid tert-butyl ester
CAS No.:676555-73-0
Molecular Formula:C₃₈H₄₉N₃O₆
Molecular Weight:643.824
Hs Code.:

6-{2-[allyloxycarbonyl-(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-amino]-acetylamino}-hexanoic acid <i>tert</i>-butyl ester

Synonyms:6-{2-[allyloxycarbonyl-(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-amino]-acetylamino}-hexanoic acid tert-butyl ester

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Chemical Property of 6-{2-[allyloxycarbonyl-(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-amino]-acetylamino}-hexanoic acid tert-butyl ester

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Technology Process of 6-{2-[allyloxycarbonyl-(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-amino]-acetylamino}-hexanoic acid tert-butyl ester

There total 3 articles about 6-{2-[allyloxycarbonyl-(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-amino]-acetylamino}-hexanoic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.0%

: 5514-98-7
6-aminohexanoic acid tert-butyl ester

: 676555-53-6
[allyloxycarbonyl-(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-amino]-acetic acid

: 676555-73-0
6-{2-[allyloxycarbonyl-(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-amino]-acetylamino}-hexanoic acid tert-butyl ester

Guidance literature:: With (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 2h;
DOI:10.1039/b311775h

Reference yield:

: 172405-21-9
methyl N-<2-((4-methoxyphenyl)-diphenylmethyl)aminoethyl> glycinate

: 676555-73-0
6-{2-[allyloxycarbonyl-(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-amino]-acetylamino}-hexanoic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 92 percent / diisopropylethylamine / CH₂Cl₂ / 20 °C

2: 92 percent / aq. LiOH; CaCl₂ / propan-2-ol / 6 h / 20 °C

3: 74 percent / diisopropylethylamine; Bop / dimethylformamide / 2 h / 0 - 20 °C

With lithium hydroxide; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; calcium chloride; In dichloromethane; N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1039/b311775h

Reference yield:

: 221554-84-3
methyl -N-glycinate

: 676555-73-0
6-{2-[allyloxycarbonyl-(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl)-amino]-acetylamino}-hexanoic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / aq. LiOH; CaCl₂ / propan-2-ol / 6 h / 20 °C

2: 74 percent / diisopropylethylamine; Bop / dimethylformamide / 2 h / 0 - 20 °C

With lithium hydroxide; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; calcium chloride; In N,N-dimethyl-formamide; isopropyl alcohol;
DOI:10.1039/b311775h