{4-[3-(4-allyloxy-3-ethyl-5-methyl-phenyl)-[1,2,4]oxadiazol-5-yl]-6-methyl-pyridin-2-yl}-dimethyl-amine

Base Information

Chemical Name:{4-[3-(4-allyloxy-3-ethyl-5-methyl-phenyl)-[1,2,4]oxadiazol-5-yl]-6-methyl-pyridin-2-yl}-dimethyl-amine
CAS No.:1062669-57-1
Molecular Formula:C₂₂H₂₆N₄O₂
Molecular Weight:378.474
Hs Code.:

Synonyms:{4-[3-(4-allyloxy-3-ethyl-5-methyl-phenyl)-[1,2,4]oxadiazol-5-yl]-6-methyl-pyridin-2-yl}-dimethyl-amine

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Chemical Property of {4-[3-(4-allyloxy-3-ethyl-5-methyl-phenyl)-[1,2,4]oxadiazol-5-yl]-6-methyl-pyridin-2-yl}-dimethyl-amine

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Technology Process of {4-[3-(4-allyloxy-3-ethyl-5-methyl-phenyl)-[1,2,4]oxadiazol-5-yl]-6-methyl-pyridin-2-yl}-dimethyl-amine

There total 6 articles about {4-[3-(4-allyloxy-3-ethyl-5-methyl-phenyl)-[1,2,4]oxadiazol-5-yl]-6-methyl-pyridin-2-yl}-dimethyl-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1062669-55-9
C₂₂H₂₈N₄O₃

: 1062669-57-1
{4-[3-(4-allyloxy-3-ethyl-5-methyl-phenyl)-[1,2,4]oxadiazol-5-yl]-6-methyl-pyridin-2-yl}-dimethyl-amine

Guidance literature:: In 1,4-dioxane; at 95 ℃; for 16h;

Reference yield:

: 1062669-55-9
C₂₂H₂₈N₄O₃

: 1062669-57-1
{4-[3-(4-allyloxy-3-ethyl-5-methyl-phenyl)-[1,2,4]oxadiazol-5-yl]-6-methyl-pyridin-2-yl}-dimethyl-amine

Guidance literature:: In 1,4-dioxane; at 95 ℃; for 16h;

Reference yield:

: 849226-45-5
2-chloro-6-methyl-isonicotinic acid tert.-butyl ester

: 1062669-57-1
{4-[3-(4-allyloxy-3-ethyl-5-methyl-phenyl)-[1,2,4]oxadiazol-5-yl]-6-methyl-pyridin-2-yl}-dimethyl-amine

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium t-butanolate / palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene / tetrahydrofuran / 18 h / 110 °C

1.2: 18 h / 100 °C

2.1: benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 20 °C

3.1: 1,4-dioxane / 16 h / 95 °C

With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; sodium t-butanolate; palladium diacetate; 4,5-bis(diphenylphosphino)-9,9-dimethylxanthene; In tetrahydrofuran; 1,4-dioxane; dichloromethane;