<(4-acetamidophenyl)aminomethane>phenylphosphinic acid

Base Information

• Chemical Name: <(4-acetamidophenyl)aminomethane>phenylphosphinic acid
• CAS No.: 131149-07-0
• Molecular Formula: C₁₅H₁₇N₂O₃P
• Molecular Weight: 304.285
• Mol file: 131149-07-0.mol

Synonyms:<(4-acetamidophenyl)aminomethane>phenylphosphinic acid

Chemical Property of <(4-acetamidophenyl)aminomethane>phenylphosphinic acid

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of <(4-acetamidophenyl)aminomethane>phenylphosphinic acid

There total 4 articles about <(4-acetamidophenyl)aminomethane>phenylphosphinic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

<(4-acetamidophenyl)allylaminomethane>phenylphosphinic acid (131479-95-3) → <(4-acetamidophenyl)aminomethane>phenylphosphinic acid (131149-07-0)

Guidance literature:

palladium on activated charcoal; In ethanol; Heating;

DOI:10.1016/S0040-4020(01)87899-6

Reference yield:

Phenylphosphonigsaeure-bis(trimethylsilylester) (63007-86-3) → <(4-acetamidophenyl)aminomethane>phenylphosphinic acid (131149-07-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 77 percent / CH₂Cl₂ / Ambient temperature

2: 95 percent / 10percent Pd-C / ethanol / Heating

palladium on activated charcoal; In ethanol; dichloromethane;

DOI:10.1016/S0040-4020(01)87899-6

Reference yield:

para-acetamidobenzaldehyde (122-85-0) → <(4-acetamidophenyl)aminomethane>phenylphosphinic acid (131149-07-0)

Guidance literature:

Multi-step reaction with 3 steps

1: CH₂Cl₂ / or in benzene

2: 77 percent / CH₂Cl₂ / Ambient temperature

3: 95 percent / 10percent Pd-C / ethanol / Heating

palladium on activated charcoal; In ethanol; dichloromethane;

DOI:10.1016/S0040-4020(01)87899-6

upstream raw materials:

<(4-acetamidophenyl)allylaminomethane>phenylphosphinic acid

Phenylphosphonigsaeure-bis(trimethylsilylester)

para-acetamidobenzaldehyde

4-acetamidobenzaldehyde N-allylimine

Refernces