1-(4-methoxyphenyl)-4-hydroxy-3-(hydroxymethyl)-6,7-dimethoxynaphthalene-2-carboxylic acid lactone

Base Information

Chemical Name:1-(4-methoxyphenyl)-4-hydroxy-3-(hydroxymethyl)-6,7-dimethoxynaphthalene-2-carboxylic acid lactone
CAS No.:116515-73-2
Molecular Formula:C₂₁H₁₈O₆
Molecular Weight:366.37
Hs Code.:

Synonyms:1-(4-methoxyphenyl)-4-hydroxy-3-(hydroxymethyl)-6,7-dimethoxynaphthalene-2-carboxylic acid lactone

Suppliers and Price of 1-(4-methoxyphenyl)-4-hydroxy-3-(hydroxymethyl)-6,7-dimethoxynaphthalene-2-carboxylic acid lactone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-(4-methoxyphenyl)-4-hydroxy-3-(hydroxymethyl)-6,7-dimethoxynaphthalene-2-carboxylic acid lactone

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-(4-methoxyphenyl)-4-hydroxy-3-(hydroxymethyl)-6,7-dimethoxynaphthalene-2-carboxylic acid lactone

There total 3 articles about 1-(4-methoxyphenyl)-4-hydroxy-3-(hydroxymethyl)-6,7-dimethoxynaphthalene-2-carboxylic acid lactone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 116515-72-1
dimethyl 4-hydroxy-6,7-dimethoxy-1-(4'-methoxyphenyl)naphthalene-2,3-dicarboxylate

: 116515-73-2
1-(4-methoxyphenyl)-4-hydroxy-3-(hydroxymethyl)-6,7-dimethoxynaphthalene-2-carboxylic acid lactone

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; methanol; Ambient temperature;

Reference yield: 69.0%

: 1621253-15-3
t-butyl 6,7-dimethoxy-9-(4-methoxyphenyl)-1-oxo-1,3-dihydronaphtho[2,3-c]furan-4-yl carbonate

: 116515-73-2
1-(4-methoxyphenyl)-4-hydroxy-3-(hydroxymethyl)-6,7-dimethoxynaphthalene-2-carboxylic acid lactone

Guidance literature:: With piperidine; In dichloromethane; at 0 - 25 ℃; for 5h;

Reference yield: 65.0%

: 1402834-01-8
diethyl 1-(4-methoxyphenyl)-4-hydroxy-6,7-dimethoxynaphthalene-2,3-dicarboxylate

: 116515-73-2
1-(4-methoxyphenyl)-4-hydroxy-3-(hydroxymethyl)-6,7-dimethoxynaphthalene-2-carboxylic acid lactone

Guidance literature:: diethyl 1-(4-methoxyphenyl)-4-hydroxy-6,7-dimethoxynaphthalene-2,3-dicarboxylate; With sodium tetrahydroborate; In methanol; at 20 ℃; for 6h; Inert atmosphere;

With hydrogenchloride; In methanol; water; for 1h; Inert atmosphere;
DOI:10.1007/s00044-012-0245-1