4-(2-(2-(trimethylsilyl)ethynyl)phenyl)but-3-ynyl 3,5-bis(benzyloxy)benzoate

Base Information

Chemical Name:4-(2-(2-(trimethylsilyl)ethynyl)phenyl)but-3-ynyl 3,5-bis(benzyloxy)benzoate
CAS No.:1268341-75-8
Molecular Formula:C₃₆H₃₄O₄Si
Molecular Weight:558.749
Hs Code.:

Synonyms:4-(2-(2-(trimethylsilyl)ethynyl)phenyl)but-3-ynyl 3,5-bis(benzyloxy)benzoate

Suppliers and Price of 4-(2-(2-(trimethylsilyl)ethynyl)phenyl)but-3-ynyl 3,5-bis(benzyloxy)benzoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(2-(2-(trimethylsilyl)ethynyl)phenyl)but-3-ynyl 3,5-bis(benzyloxy)benzoate

Chemical Property:

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Technology Process of 4-(2-(2-(trimethylsilyl)ethynyl)phenyl)but-3-ynyl 3,5-bis(benzyloxy)benzoate

There total 6 articles about 4-(2-(2-(trimethylsilyl)ethynyl)phenyl)but-3-ynyl 3,5-bis(benzyloxy)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 28917-43-3
3,5-dibenzyloxybenzoic acid

: 159305-97-2
4-<2-<(Trimethylsilyl)ethynyl>phenyl>-3-butyn-1-ol

: 1268341-75-8
4-(2-(2-(trimethylsilyl)ethynyl)phenyl)but-3-ynyl 3,5-bis(benzyloxy)benzoate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1002/pola.24556

Reference yield:

: 2150-44-9
1-carbomethoxy-3,5-dihydroxybenzene

: 1268341-75-8
4-(2-(2-(trimethylsilyl)ethynyl)phenyl)but-3-ynyl 3,5-bis(benzyloxy)benzoate

Guidance literature:: Multi-step reaction with 3 steps

1: 18-crown-6 ether; potassium carbonate / acetone / 48 °C / Inert atmosphere; Reflux

2: potassium hydroxide / tetrahydrofuran; methanol; water / Reflux

3: dmap; dicyclohexyl-carbodiimide / dichloromethane / 24 h / 20 °C / Inert atmosphere

With dmap; 18-crown-6 ether; potassium carbonate; dicyclohexyl-carbodiimide; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; acetone;
DOI:10.1002/pola.24556

Reference yield:

: 58605-10-0
methyl 3,5-bis(benzyloxy)benzoate

: 1268341-75-8
4-(2-(2-(trimethylsilyl)ethynyl)phenyl)but-3-ynyl 3,5-bis(benzyloxy)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium hydroxide / tetrahydrofuran; methanol; water / Reflux

2: dmap; dicyclohexyl-carbodiimide / dichloromethane / 24 h / 20 °C / Inert atmosphere

With dmap; dicyclohexyl-carbodiimide; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1002/pola.24556