3,4,6,7-tetra-O-benzyl-2-O-acetyl-L-glycero-α/β-D-manno-heptapyranoside trichloroacetimidate

Base Information

• Chemical Name: 3,4,6,7-tetra-O-benzyl-2-O-acetyl-L-glycero-α/β-D-manno-heptapyranoside trichloroacetimidate
• CAS No.: 1021393-82-7
• Molecular Formula: C₃₉H₄₀Cl₃NO₈
• Molecular Weight: 757.107

Synonyms:3,4,6,7-tetra-O-benzyl-2-O-acetyl-L-glycero-α/β-D-manno-heptapyranoside trichloroacetimidate

Chemical Property of 3,4,6,7-tetra-O-benzyl-2-O-acetyl-L-glycero-α/β-D-manno-heptapyranoside trichloroacetimidate

Chemical Property:

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Technology Process of 3,4,6,7-tetra-O-benzyl-2-O-acetyl-L-glycero-α/β-D-manno-heptapyranoside trichloroacetimidate

There total 1 articles about 3,4,6,7-tetra-O-benzyl-2-O-acetyl-L-glycero-α/β-D-manno-heptapyranoside trichloroacetimidate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

3,4,6,7-tetra-O-benzyl-2-O-acetyl-L-glycero-α/β-D-manno-heptapyranoside + trichloroacetonitrile (545-06-2) → 3,4,6,7-tetra-O-benzyl-2-O-acetyl-L-glycero-α/β-D-manno-heptapyranoside trichloroacetimidate (1021393-82-7)

Guidance literature:

3,4,6,7-tetra-O-benzyl-2-O-acetyl-L-glycero-α/β-D-manno-heptapyranoside; trichloroacetonitrile; In dichloromethane; at 20 ℃; for 0.166667h; Molecular sieve;

With caesium carbonate; In dichloromethane; at 20 ℃; for 0.75h;

DOI:10.1002/anie.200704262

upstream raw materials:

trichloroacetonitrile

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