C₁₆H₁₆O₂

Base Information

Chemical Name:C₁₆H₁₆O₂
CAS No.:1415560-52-9
Molecular Formula:C₁₆H₁₆O₂
Molecular Weight:240.302
Hs Code.:

C<sub>16</sub>H<sub>16</sub>O<sub>2</sub>

Synonyms:C₁₆H₁₆O₂

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Chemical Property of C₁₆H₁₆O₂

Chemical Property:

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Technology Process of C₁₆H₁₆O₂

There total 8 articles about C₁₆H₁₆O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 6336-45-4
vinylboronic acid dibutyl ester

: 1415560-26-7
C₁₆H₁₈O₃

: 1415560-52-9
C₁₆H₁₆O₂

Guidance literature:: With (R)-3,3'-dibromo-1,1'-bi-2-naphthol; In toluene; at 80 ℃; for 12h; enantioselective reaction; Inert atmosphere;
DOI:10.1021/ja309076g

Reference yield:

: 1415560-39-2
(S,E)-2-(1,3-diphenylallyl)-5-methoxyphenol

: 1415560-52-9
C₁₆H₁₆O₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium carbonate / acetone / 0.25 h / Inert atmosphere

1.2: 35 h / 20 °C / Inert atmosphere; Reflux

2.1: osmium(VIII) oxide; 4-methylmorpholine N-oxide; water / acetone; tert-butyl alcohol / 0.33 h / 20 °C / Inert atmosphere

3.1: lead(IV) tetraacetate / dichloromethane / 2 h / 0 - 20 °C

4.1: n-butyllithium / tetrahydrofuran / 0.17 h / 0 °C / Inert atmosphere

4.2: 1 h / 0 - 20 °C / Inert atmosphere

5.1: dimethylsulfide borane complex / tetrahydrofuran / Inert atmosphere

6.1: dihydrogen peroxide; sodium hydroxide / Inert atmosphere

7.1: boron tribromide / Inert atmosphere

With osmium(VIII) oxide; n-butyllithium; dimethylsulfide borane complex; water; dihydrogen peroxide; lead(IV) tetraacetate; boron tribromide; potassium carbonate; 4-methylmorpholine N-oxide; sodium hydroxide; In tetrahydrofuran; dichloromethane; acetone; tert-butyl alcohol;
DOI:10.1021/ja309076g

Reference yield:

: C₂₃H₂₄O₄

: 1415560-52-9
C₁₆H₁₆O₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: lead(IV) tetraacetate / dichloromethane / 2 h / 0 - 20 °C

2.1: n-butyllithium / tetrahydrofuran / 0.17 h / 0 °C / Inert atmosphere

2.2: 1 h / 0 - 20 °C / Inert atmosphere

3.1: dimethylsulfide borane complex / tetrahydrofuran / Inert atmosphere

4.1: dihydrogen peroxide; sodium hydroxide / Inert atmosphere

5.1: boron tribromide / Inert atmosphere

With n-butyllithium; dimethylsulfide borane complex; dihydrogen peroxide; lead(IV) tetraacetate; boron tribromide; sodium hydroxide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja309076g