ethyl (3S)-3-(4-(tetrahydro-2H-pyran-2-yloxy)phenyl)-5-(tributylstannanyl)-4-E-pentenoate

Base Information

• Chemical Name: ethyl (3S)-3-(4-(tetrahydro-2H-pyran-2-yloxy)phenyl)-5-(tributylstannanyl)-4-E-pentenoate
• CAS No.: 1012070-62-0
• Molecular Formula: C₃₀H₅₀O₄Sn
• Molecular Weight: 593.435

Synonyms:ethyl (3S)-3-(4-(tetrahydro-2H-pyran-2-yloxy)phenyl)-5-(tributylstannanyl)-4-E-pentenoate

Chemical Property of ethyl (3S)-3-(4-(tetrahydro-2H-pyran-2-yloxy)phenyl)-5-(tributylstannanyl)-4-E-pentenoate

Chemical Property:

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Technology Process of ethyl (3S)-3-(4-(tetrahydro-2H-pyran-2-yloxy)phenyl)-5-(tributylstannanyl)-4-E-pentenoate

There total 3 articles about ethyl (3S)-3-(4-(tetrahydro-2H-pyran-2-yloxy)phenyl)-5-(tributylstannanyl)-4-E-pentenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C18H22O4 (1012070-60-8) + tri-n-butyl-tin hydride (688-73-3) → ethyl (3S)-3-(4-(tetrahydro-2H-pyran-2-yloxy)phenyl)-5-(tributylstannanyl)-4-E-pentenoate (1012070-62-0) + C30H50O4Sn (1012071-28-1)

Guidance literature:

bis-triphenylphosphine-palladium(II) chloride; In tetrahydrofuran; for 0.0333333h;

Reference yield:

3,4-dihydro-2H-pyran (110-87-2) → ethyl (3S)-3-(4-(tetrahydro-2H-pyran-2-yloxy)phenyl)-5-(tributylstannanyl)-4-E-pentenoate (1012070-62-0) + C30H50O4Sn (1012071-28-1)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridinium p-toluenesulfonate / dichloromethane / 16 h / 23 °C

2: bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran / 0.03 h

bis-triphenylphosphine-palladium(II) chloride; pyridinium p-toluenesulfonate; In tetrahydrofuran; dichloromethane;

Reference yield:

C13H14O3 (1012071-27-0) → ethyl (3S)-3-(4-(tetrahydro-2H-pyran-2-yloxy)phenyl)-5-(tributylstannanyl)-4-E-pentenoate (1012070-62-0) + C30H50O4Sn (1012071-28-1)

Guidance literature:

Multi-step reaction with 2 steps

1: pyridinium p-toluenesulfonate / dichloromethane / 16 h / 23 °C

2: bis-triphenylphosphine-palladium(II) chloride / tetrahydrofuran / 0.03 h

bis-triphenylphosphine-palladium(II) chloride; pyridinium p-toluenesulfonate; In tetrahydrofuran; dichloromethane;

upstream raw materials:

C₁₈H₂₂O₄

tri-n-butyl-tin hydride

3,4-dihydro-2H-pyran

C₁₃H₁₄O₃

Downstream raw materials:

ethyl (3S,4E)-3-(4-(((2'-(butyloxy)-6-(1,1-dimethylethyl)-5'-(methyloxy)-1,1'-biphenyl-3-yl)methyl)oxy)phenyl)-4-hexenoate

ethyl (3S,4E)-3-(4-(((6-(1,1-dimethylethyl)-2'-fluoro-5'-(methyloxy)-1,1'-biphenyl-3-yl)methyl)oxy)phenyl)-4-heptenoate

ethyl (3S,4E)-3-(4-(((6-(1,1-dimethylethyl)-2'-fluoro-5'-(methyloxy)-1,1'-biphenyl-3-yl)methyl)oxy)phenyl)-4-hexenoate

(3S,4E)-3-(4-(((6-(1,1-dimethylethyl)-2'-fluoro-5'-(methyloxy)-1,1'-biphenyl-3-yl)methyl)oxy)phenyl)-4-heptenoic acid

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