benzyl 2-acetamido-3-O-benzyl-2,4,6-trideoxy-4,6-difluoro-α-D-galactopyranoside

Base Information

Chemical Name:benzyl 2-acetamido-3-O-benzyl-2,4,6-trideoxy-4,6-difluoro-α-D-galactopyranoside
CAS No.:129728-83-2
Molecular Formula:C₂₂H₂₅F₂NO₄
Molecular Weight:405.442
Hs Code.:

Synonyms:benzyl 2-acetamido-3-O-benzyl-2,4,6-trideoxy-4,6-difluoro-α-D-galactopyranoside

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Chemical Property of benzyl 2-acetamido-3-O-benzyl-2,4,6-trideoxy-4,6-difluoro-α-D-galactopyranoside

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Technology Process of benzyl 2-acetamido-3-O-benzyl-2,4,6-trideoxy-4,6-difluoro-α-D-galactopyranoside

There total 5 articles about benzyl 2-acetamido-3-O-benzyl-2,4,6-trideoxy-4,6-difluoro-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 38660-64-9
benzyl 2-acetamido-3-O-benzyl-2-deoxy-4,6-di-O-mesyl-α-D-glucopyranoside

: 129728-83-2
benzyl 2-acetamido-3-O-benzyl-2,4,6-trideoxy-4,6-difluoro-α-D-galactopyranoside

Guidance literature:: With tetrabutyl ammonium fluoride; In acetonitrile; for 112h; Heating;
DOI:10.1016/0008-6215(90)84293-4

Reference yield:

: 14146-26-0
benzyl 2-acetamido-3-O-benzyl-4,6-O-benzylidene-2-deoxy-α-D-glucopyranoside

: 129728-83-2
benzyl 2-acetamido-3-O-benzyl-2,4,6-trideoxy-4,6-difluoro-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / aq. acetic acid / 1.5 h / 90 - 100 °C

2: 78 percent / pyridine / 0 - 5 °C

3: 88 percent / tetrabutylammonium fluoride / acetonitrile / 112 h / Heating

With pyridine; tetrabutyl ammonium fluoride; acetic acid; In acetonitrile;
DOI:10.1016/0008-6215(90)84293-4

Reference yield:

: 14146-27-1
benzyl 3-O-benzyl-2-acetamido-2-deoxy-α-D-glucopyranoside

: 129728-83-2
benzyl 2-acetamido-3-O-benzyl-2,4,6-trideoxy-4,6-difluoro-α-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / pyridine / 0 - 5 °C

2: 88 percent / tetrabutylammonium fluoride / acetonitrile / 112 h / Heating

With pyridine; tetrabutyl ammonium fluoride; In acetonitrile;
DOI:10.1016/0008-6215(90)84293-4