C₂₂H₃₂N₂O₈Si

Base Information

• Chemical Name: C₂₂H₃₂N₂O₈Si
• CAS No.: 501347-42-8
• Molecular Formula: C₂₂H₃₂N₂O₈Si
• Molecular Weight: 480.59
• Mol file: 501347-42-8.mol

Synonyms:C₂₂H₃₂N₂O₈Si

Chemical Property of C₂₂H₃₂N₂O₈Si

Chemical Property:

Purity/Quality:

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Technology Process of C₂₂H₃₂N₂O₈Si

There total 1 articles about C₂₂H₃₂N₂O₈Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

ortho-nitrofluorobenzene (1493-27-2,127723-77-7) + C16H29NO6Si (319491-85-5) → C22H32N2O8Si (501347-42-8)

Guidance literature:

With potassium tert-butylate; In N,N-dimethyl-formamide; at 20 ℃;

DOI:10.1021/ol020229e

Reference yield: 48.0%

C22H32N2O8Si (501347-42-8) → C16H18N2O8 (501347-43-9)

Guidance literature:

With triethylamine hydrofluoride; In tetrahydrofuran; at 20 ℃; for 144h;

DOI:10.1021/ol020229e

Reference yield:

C22H32N2O8Si (501347-42-8) → C16H16N2O8

Guidance literature:

Multi-step reaction with 2 steps

1: 48 percent / Et₃N*HF / tetrahydrofuran / 144 h / 20 °C

2: 89 percent / pyridinium dichromate; acetic acid / CH₂Cl₂ / 20 °C

With dipyridinium dichromate; acetic acid; triethylamine hydrofluoride; In tetrahydrofuran; dichloromethane;

DOI:10.1021/ol020229e

upstream raw materials:

ortho-nitrofluorobenzene

C₁₆H₂₉NO₆Si

Downstream raw materials:

C₁₆H₁₈N₂O₈