dodecyl 4,6-O-benzylidene-2,3-bis-[2-(2-chloroacetamido)ethyl]-β-D-galactopyranoside

Base Information

Chemical Name:dodecyl 4,6-O-benzylidene-2,3-bis-[2-(2-chloroacetamido)ethyl]-β-D-galactopyranoside
CAS No.:1427214-14-9
Molecular Formula:C₃₃H₅₂Cl₂N₂O₈
Molecular Weight:675.69
Hs Code.:

Synonyms:dodecyl 4,6-O-benzylidene-2,3-bis-[2-(2-chloroacetamido)ethyl]-β-D-galactopyranoside

Suppliers and Price of dodecyl 4,6-O-benzylidene-2,3-bis-[2-(2-chloroacetamido)ethyl]-β-D-galactopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of dodecyl 4,6-O-benzylidene-2,3-bis-[2-(2-chloroacetamido)ethyl]-β-D-galactopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of dodecyl 4,6-O-benzylidene-2,3-bis-[2-(2-chloroacetamido)ethyl]-β-D-galactopyranoside

There total 7 articles about dodecyl 4,6-O-benzylidene-2,3-bis-[2-(2-chloroacetamido)ethyl]-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 1427214-12-7
dodecyl 4,6-O-benzylidene-2,3-bis-(2-aminoethyl)-β-D-galactopyranoside

: 541-88-8
Chloroacetic anhydride

: 1427214-14-9
dodecyl 4,6-O-benzylidene-2,3-bis-[2-(2-chloroacetamido)ethyl]-β-D-galactopyranoside

Guidance literature:: In dichloromethane; at 0 - 20 ℃;
DOI:10.1016/j.tetlet.2013.01.025

Reference yield:

: 4163-60-4
β-D-galactose peracetate

: 1427214-14-9
dodecyl 4,6-O-benzylidene-2,3-bis-[2-(2-chloroacetamido)ethyl]-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 6 steps

1.1: boron trifluoride diethyl etherate / dichloromethane / 5 h / 20 °C

2.1: sodium methylate / methanol / 4 h

3.1: toluene-4-sulfonic acid / dichloromethane

4.1: tetra(n-butyl)ammonium hydrogensulfate; sodium hydroxide / toluene; water / 0.5 h / 10 °C

4.2: 2 h

5.1: lithium aluminium tetrahydride / tetrahydrofuran / 1.5 h / 0 °C

6.1: dichloromethane / 0 - 20 °C

With lithium aluminium tetrahydride; boron trifluoride diethyl etherate; sodium methylate; tetra(n-butyl)ammonium hydrogensulfate; toluene-4-sulfonic acid; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; toluene;
DOI:10.1016/j.tetlet.2013.01.025

Reference yield:

: 1427214-10-5
dodecyl 4,6-O-benzylidene-2,3-bis-O-[cyanomethyl]-β-D-galactopyranoside//

: 1427214-14-9
dodecyl 4,6-O-benzylidene-2,3-bis-[2-(2-chloroacetamido)ethyl]-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 1.5 h / 0 °C

2: dichloromethane / 0 - 20 °C

With lithium aluminium tetrahydride; In tetrahydrofuran; dichloromethane;
DOI:10.1016/j.tetlet.2013.01.025