4-[bis-(4-hydroxy-phenyl)-methylene]-cyclohexanecarboxylic acid ethyl ester

Base Information

Chemical Name:4-[bis-(4-hydroxy-phenyl)-methylene]-cyclohexanecarboxylic acid ethyl ester
CAS No.:886587-61-7
Molecular Formula:C₂₂H₂₄O₄
Molecular Weight:352.43
Hs Code.:

Synonyms:4-[bis-(4-hydroxy-phenyl)-methylene]-cyclohexanecarboxylic acid ethyl ester

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Chemical Property of 4-[bis-(4-hydroxy-phenyl)-methylene]-cyclohexanecarboxylic acid ethyl ester

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Technology Process of 4-[bis-(4-hydroxy-phenyl)-methylene]-cyclohexanecarboxylic acid ethyl ester

There total 1 articles about 4-[bis-(4-hydroxy-phenyl)-methylene]-cyclohexanecarboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 611-99-4
4,4'-Dihydroxybenzophenone

: 17159-79-4
ethyl 4-oxocyclohexane-1-carboxylate

: 886587-61-7
4-[bis-(4-hydroxy-phenyl)-methylene]-cyclohexanecarboxylic acid ethyl ester

Guidance literature:: With titanium tetrachloride; zinc; In tetrahydrofuran; for 2h; Heating;
DOI:10.1021/jm0512037

Reference yield: 95.0%

: 886587-61-7
4-[bis-(4-hydroxy-phenyl)-methylene]-cyclohexanecarboxylic acid ethyl ester

: 107-30-2
chloromethyl methyl ether

: 886587-63-9
ethyl 4-[bis(4-methoxymethoxyphenyl)methylene]cyclohexanecarboxylate

Guidance literature:: 4-[bis-(4-hydroxy-phenyl)-methylene]-cyclohexanecarboxylic acid ethyl ester; With sodium hydride; In N,N-dimethyl-formamide; cooling;

chloromethyl methyl ether; In N,N-dimethyl-formamide; at 20 ℃; for 1h;
DOI:10.1021/jm0512037

Reference yield:

: 886587-61-7
4-[bis-(4-hydroxy-phenyl)-methylene]-cyclohexanecarboxylic acid ethyl ester

: 886587-99-1
4-fluoromethyl[bis(4-methoxymethoxyphenyl)methylene]cyclohexane

Guidance literature:: Multi-step reaction with 4 steps

1.1: sodium hydride / dimethylformamide / cooling

1.2: 95 percent / dimethylformamide / 1 h / 20 °C

2.1: 89 percent / LiAlH₄ / tetrahydrofuran / 1 h / 20 °C

3.1: 95 percent / triethylamine / CH₂Cl₂ / 1 h / 20 °C

4.1: 63 percent / cesium fluoride; 1-butyl-3-methylimidazolium tetrafluoroboronate; H₂O / acetonitrile

With lithium aluminium tetrahydride; water; sodium hydride; triethylamine; cesium fluoride; 1-butyl-3-methylimidazolium Tetrafluoroborate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm0512037