15-(tert-Butyl-diphenyl-silanyloxy)-16-oxo-hexadecanoic acid methyl ester

Base Information

Chemical Name:15-(tert-Butyl-diphenyl-silanyloxy)-16-oxo-hexadecanoic acid methyl ester
CAS No.:110815-11-7
Molecular Formula:C₃₃H₅₀O₄Si
Molecular Weight:538.843
Hs Code.:

Synonyms:15-(tert-Butyl-diphenyl-silanyloxy)-16-oxo-hexadecanoic acid methyl ester

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Chemical Property of 15-(tert-Butyl-diphenyl-silanyloxy)-16-oxo-hexadecanoic acid methyl ester

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Technology Process of 15-(tert-Butyl-diphenyl-silanyloxy)-16-oxo-hexadecanoic acid methyl ester

There total 2 articles about 15-(tert-Butyl-diphenyl-silanyloxy)-16-oxo-hexadecanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 76529-42-5
methyl 15-hydroxypentadecanoate

: 110815-11-7
15-(tert-Butyl-diphenyl-silanyloxy)-16-oxo-hexadecanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) (COCl)2, DMSO, Et₃N / 1.) methylene dichloride, 2.) THF, 0 grad C

2: 1.) imidazole, 2.) O₃ / 1.) DMF, 2.) methylene dichloride

With 1H-imidazole; oxalyl dichloride; ozone; dimethyl sulfoxide; triethylamine;
DOI:10.1016/S0040-4039(00)85302-2

Reference yield:

: 110815-10-6
15-Hydroxy-heptadec-16-enoic acid methyl ester

: 58479-61-1
tert-butylchlorodiphenylsilane

: 110815-11-7
15-(tert-Butyl-diphenyl-silanyloxy)-16-oxo-hexadecanoic acid methyl ester

Guidance literature:: With 1H-imidazole; ozone; Yield given. Multistep reaction; 1.) DMF, 2.) methylene dichloride;
DOI:10.1016/S0040-4039(00)85302-2