C₃₀H₄₈O₆Si

Base Information

Chemical Name:C₃₀H₄₈O₆Si
CAS No.:934560-36-8
Molecular Formula:C₃₀H₄₈O₆Si
Molecular Weight:532.793
Hs Code.:

C<sub>30</sub>H<sub>48</sub>O<sub>6</sub>Si

Synonyms:C₃₀H₄₈O₆Si

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Chemical Property of C₃₀H₄₈O₆Si

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Technology Process of C₃₀H₄₈O₆Si

There total 7 articles about C₃₀H₄₈O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: C₂₉H₄₈O₅Si

: 107-02-8,25068-14-8
acrolein

: 934560-36-8
C₃₀H₄₈O₆Si

Guidance literature:: [(N,N-dimesityl-diazol-1-ium-2-yl)(Cl)2Ru=CH(2-i-PrO)Ph]; In dichloromethane; for 12h; Heating;
DOI:10.1039/b616558c

Reference yield:

: 863659-96-5
2-Methyl-2-[(2R,6S)-6-(2-oxo-ethyl)-tetrahydro-pyran-2-yl]-propionic acid methyl ester

: 934560-36-8
C₃₀H₄₈O₆Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: (+)-DIPBr / tetrahydrofuran / -78 °C

2.1: 89 percent / NaH / dimethylformamide / 0.5 h / 0 °C

3.1: 83 percent / Ti[O-(i-Pr)]4 / 48 h / Heating

4.1: osmium tetraoxide; NMO / 12 h

4.2: 90 percent / NaIO₄ / 0.5 h

5.1: 78 percent / n-BuLi; KOt-Bu; B(^dIpc)2OMe / BF₃*OEt₂ / -78 °C

6.1: 79 percent / [(N,N-dimesityl-diazol-1-ium-2-yl)(Cl)2Ru=CH(2-i-PrO)Ph] / CH₂Cl₂ / 12 h / Heating

With osmium(VIII) oxide; n-butyllithium; N-methyl-2-indolinone; B(^dIpc)2OMe; potassium tert-butylate; sodium hydride; boron trifluoride diethyl etherate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 1.1: Brown allylation / 5.1: Brown crotylation;
DOI:10.1039/b616558c

Reference yield:

: C₁₉H₂₇O₄Br

: 934560-36-8
C₃₀H₄₈O₆Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: H₂; NaHCO₃ / Pd/C / 24 h

1.2: Dess-Martin periodinane / CH₂Cl₂ / 0.5 h / 0 °C

2.1: (+)-DIPBr / tetrahydrofuran / -78 °C

3.1: 89 percent / NaH / dimethylformamide / 0.5 h / 0 °C

4.1: 83 percent / Ti[O-(i-Pr)]4 / 48 h / Heating

5.1: osmium tetraoxide; NMO / 12 h

5.2: 90 percent / NaIO₄ / 0.5 h

6.1: 78 percent / n-BuLi; KOt-Bu; B(^dIpc)2OMe / BF₃*OEt₂ / -78 °C

7.1: 79 percent / [(N,N-dimesityl-diazol-1-ium-2-yl)(Cl)2Ru=CH(2-i-PrO)Ph] / CH₂Cl₂ / 12 h / Heating

With osmium(VIII) oxide; n-butyllithium; N-methyl-2-indolinone; B(^dIpc)2OMe; potassium tert-butylate; hydrogen; sodium hydride; sodium hydrogencarbonate; palladium on activated charcoal; boron trifluoride diethyl etherate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 1.2: Dess-Martin oxidation / 2.1: Brown allylation / 6.1: Brown crotylation;
DOI:10.1039/b616558c