Technology Process of C40H36BrNO6
There total 15 articles about C40H36BrNO6 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
N-Bromosuccinimide;
In
dichloromethane;
at 0 - 20 ℃;
for 12h;
chemoselective reaction;
Darkness;
DOI:10.1021/jo400841d
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium carbonate; Iodine monochloride / water; diethyl ether / 6 h / 0 °C / Darkness
2.1: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / tetrahydrofuran / 24 h / 65 °C / Inert atmosphere
3.1: potassium hydroxide / N,N-dimethyl-formamide / 0.5 h / 20 °C
3.2: 24 h / 50 °C
4.1: N-Bromosuccinimide / dichloromethane / 12 h / 0 - 20 °C / Darkness
With
N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium(0); Iodine monochloride; sodium carbonate; potassium carbonate; potassium hydroxide;
In
tetrahydrofuran; diethyl ether; dichloromethane; water; N,N-dimethyl-formamide;
2.1: |Larock Annulation;
DOI:10.1021/jo400841d
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: potassium carbonate; tetrakis(triphenylphosphine) palladium(0) / tetrahydrofuran / 24 h / 65 °C / Inert atmosphere
2.1: potassium hydroxide / N,N-dimethyl-formamide / 0.5 h / 20 °C
2.2: 24 h / 50 °C
3.1: N-Bromosuccinimide / dichloromethane / 12 h / 0 - 20 °C / Darkness
With
N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium(0); potassium carbonate; potassium hydroxide;
In
tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
1.1: |Larock Annulation;
DOI:10.1021/jo400841d
