3-<4-<2-<2-(3-hydroxymethylphenoxy)-3,4-dimethoxyphenyl>ethyl>phenoxy>-4,5-dimethoxybenzyl alcohol

Base Information

Chemical Name:3-<4-<2-<2-(3-hydroxymethylphenoxy)-3,4-dimethoxyphenyl>ethyl>phenoxy>-4,5-dimethoxybenzyl alcohol
CAS No.:135303-97-8
Molecular Formula:C₃₂H₃₄O₈
Molecular Weight:546.617
Hs Code.:

Synonyms:3-<4-<2-<2-(3-hydroxymethylphenoxy)-3,4-dimethoxyphenyl>ethyl>phenoxy>-4,5-dimethoxybenzyl alcohol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-<4-<2-<2-(3-hydroxymethylphenoxy)-3,4-dimethoxyphenyl>ethyl>phenoxy>-4,5-dimethoxybenzyl alcohol

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Technology Process of 3-<4-<2-<2-(3-hydroxymethylphenoxy)-3,4-dimethoxyphenyl>ethyl>phenoxy>-4,5-dimethoxybenzyl alcohol

There total 11 articles about 3-<4-<2-<2-(3-hydroxymethylphenoxy)-3,4-dimethoxyphenyl>ethyl>phenoxy>-4,5-dimethoxybenzyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 135303-96-7
methyl 3-<4-<2-<3,4-dimethoxy-2-(3-methoxycarbonylphenoxy)phenyl>ethyl>phenoxy>-4,5-dimethoxybenzoate

: 135303-97-8
3-<4-<2-<2-(3-hydroxymethylphenoxy)-3,4-dimethoxyphenyl>ethyl>phenoxy>-4,5-dimethoxybenzyl alcohol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran;

Reference yield:

: 55171-60-3
2-bromo-3,4-dimethoxybenzylaldehyde

: 135303-97-8
3-<4-<2-<2-(3-hydroxymethylphenoxy)-3,4-dimethoxyphenyl>ethyl>phenoxy>-4,5-dimethoxybenzyl alcohol

Guidance literature:: Multi-step reaction with 7 steps

1: 22 percent / K₂CO₃, cupric oxide / pyridine / 48 h / Heating

2: 95 percent / NaBH₄ / ethanol

3: PBr₃ / benzene / 2 h

4: acetonitrile / 2 h / Heating

5: 57 percent / MeONa / methanol

6: 96 percent / H₂ / Pd/C / ethyl acetate; ethanol

7: 91 percent / LiAlH₄ / tetrahydrofuran

With sodium tetrahydroborate; lithium aluminium tetrahydride; hydrogen; sodium methylate; phosphorus tribromide; potassium carbonate; copper(II) oxide; palladium on activated charcoal; In tetrahydrofuran; pyridine; methanol; ethanol; ethyl acetate; acetonitrile; benzene;

Reference yield:

: 19438-10-9
methyl 3-hydroxybenzoate

: 135303-97-8
3-<4-<2-<2-(3-hydroxymethylphenoxy)-3,4-dimethoxyphenyl>ethyl>phenoxy>-4,5-dimethoxybenzyl alcohol

Guidance literature:: Multi-step reaction with 7 steps

1: 22 percent / K₂CO₃, cupric oxide / pyridine / 48 h / Heating

2: 95 percent / NaBH₄ / ethanol

3: PBr₃ / benzene / 2 h

4: acetonitrile / 2 h / Heating

5: 57 percent / MeONa / methanol

6: 96 percent / H₂ / Pd/C / ethyl acetate; ethanol

7: 91 percent / LiAlH₄ / tetrahydrofuran

With sodium tetrahydroborate; lithium aluminium tetrahydride; hydrogen; sodium methylate; phosphorus tribromide; potassium carbonate; copper(II) oxide; palladium on activated charcoal; In tetrahydrofuran; pyridine; methanol; ethanol; ethyl acetate; acetonitrile; benzene;