1-[(2S)-2,3-dihydroxy-2,3-isopropylidenepropoxy]-2-[(2R)-2,3-epoxypropoxy]benzene

Base Information

• Chemical Name: 1-[(2S)-2,3-dihydroxy-2,3-isopropylidenepropoxy]-2-[(2R)-2,3-epoxypropoxy]benzene
• CAS No.: 248270-95-3
• Molecular Formula: C₁₅H₂₀O₅
• Molecular Weight: 280.321

Synonyms:1-[(2S)-2,3-dihydroxy-2,3-isopropylidenepropoxy]-2-[(2R)-2,3-epoxypropoxy]benzene

Chemical Property of 1-[(2S)-2,3-dihydroxy-2,3-isopropylidenepropoxy]-2-[(2R)-2,3-epoxypropoxy]benzene

Chemical Property:

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Technology Process of 1-[(2S)-2,3-dihydroxy-2,3-isopropylidenepropoxy]-2-[(2R)-2,3-epoxypropoxy]benzene

There total 6 articles about 1-[(2S)-2,3-dihydroxy-2,3-isopropylidenepropoxy]-2-[(2R)-2,3-epoxypropoxy]benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

(R)-glycidyl tosylate (113826-06-5,6746-81-2) + 1-[(2S)-2,3-dihydroxy-2,3-isopropylidenepropoxy]-2-hydroxybenzene (248270-91-9) → 1-[(2S)-2,3-dihydroxy-2,3-isopropylidenepropoxy]-2-[(2R)-2,3-epoxypropoxy]benzene (248270-95-3)

Guidance literature:

With sodium hydride; In N,N-dimethyl-formamide; at 20 ℃; for 72h;

DOI:10.1021/jo990772h

Reference yield:

(R)-glycidyl tosylate (113826-06-5,6746-81-2) + 1-[(2S)-2,3-dihydroxy-2,3-isopropylidenepropoxy]-2-hydroxybenzene (248270-91-9) → 1-[(2S)-2,3-dihydroxy-2,3-isopropylidenepropoxy]-2-[(2S)-2,3-epoxypropoxy]benzene + 1-[(2S)-2,3-dihydroxy-2,3-isopropylidenepropoxy]-2-[(2R)-2,3-epoxypropoxy]benzene (248270-95-3)

Guidance literature:

With sodium hydroxide; tetrabutylammomium bromide; In hexane; water; at 40 ℃; for 12h;

DOI:10.1021/jo990772h

Reference yield:

(R)-glycidyl tosylate (113826-06-5,6746-81-2) + 1-[(2S)-2,3-dihydroxy-2,3-isopropylidenepropoxy]-2-hydroxybenzene (248270-91-9) → 1-[(2S)-2,3-dihydroxy-2,3-isopropylidenepropoxy]-2-[(2R)-2,3-epoxypropoxy]benzene (248270-95-3) + 1-[(2R)-2,3-dihydroxy-2,3-isopropylidenepropoxy]-2-[(2R)-2,3-epoxypropoxy]benzene

Guidance literature:

With sodium hydroxide; tetrabutylammomium bromide; In hexane; water; at 40 ℃; for 12h;

DOI:10.1021/jo990772h

upstream raw materials:

(R)-glycidyl tosylate

1-[(2S)-2,3-dihydroxy-2,3-isopropylidenepropoxy]-2-hydroxybenzene

benzene-1,2-diol

(4S)-methanesulfonic acid 2,2-dimethyl-[1,3]dioxolan-4-ylmethyl ester

Downstream raw materials:

1-[(2R)-2,3-dihydroxy-3-(p-toluenesulfonyl)propoxy]-2-[(2R)-2-hydroxy-5-(triethylsilyl)pent-4-ynoxy]benzene

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