3'-O-azidomethyl-N²-benzoyl-2',5'-bis-O-tert-butyldimethylsilylguanosine

Base Information

Chemical Name:3'-O-azidomethyl-N²-benzoyl-2',5'-bis-O-tert-butyldimethylsilylguanosine
CAS No.:329032-97-5
Molecular Formula:C₃₀H₄₆N₈O₆Si₂
Molecular Weight:670.916
Hs Code.:

3'-O-azidomethyl-N<sup>2</sup>-benzoyl-2',5'-bis-O-tert-butyldimethylsilylguanosine

Synonyms:3'-O-azidomethyl-N²-benzoyl-2',5'-bis-O-tert-butyldimethylsilylguanosine

Suppliers and Price of 3'-O-azidomethyl-N²-benzoyl-2',5'-bis-O-tert-butyldimethylsilylguanosine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3'-O-azidomethyl-N²-benzoyl-2',5'-bis-O-tert-butyldimethylsilylguanosine

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Technology Process of 3'-O-azidomethyl-N²-benzoyl-2',5'-bis-O-tert-butyldimethylsilylguanosine

There total 2 articles about 3'-O-azidomethyl-N²-benzoyl-2',5'-bis-O-tert-butyldimethylsilylguanosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: N-{9-[3-(tert-butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-4-chloromethoxy-tetrahydro-furan-2-yl]-6-oxo-6,9-dihydro-1H-purin-2-yl}-benzamide

: 329032-97-5
3'-O-azidomethyl-N²-benzoyl-2',5'-bis-O-tert-butyldimethylsilylguanosine

Guidance literature:: With lithium azide; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;
DOI:10.1080/15257770008045472

Reference yield:

: 292042-78-5
N-{9-[3-(tert-butyl-dimethyl-silanyloxy)-5-(tert-butyl-dimethyl-silanyloxymethyl)-4-methylsulfanylmethoxy-tetrahydro-furan-2-yl]-6-oxo-6,9-dihydro-1H-purin-2-yl}-benzamide

: 329032-97-5
3'-O-azidomethyl-N²-benzoyl-2',5'-bis-O-tert-butyldimethylsilylguanosine

Guidance literature:: Multi-step reaction with 2 steps

1: SO₂Cl₂ / 1,2-dichloro-ethane / 0 °C

2: 250 mg / LiN₃ / dimethylformamide / 0.5 h / 20 °C

With sulfuryl dichloride; lithium azide; In 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1080/15257770008045472