3,4,6-tri-O-benzoyl-1,2-O-[(2-acrylamidoethoxy)phenylmethylene]-β-D-mannopyranoside

Base Information

Chemical Name:3,4,6-tri-O-benzoyl-1,2-O-[(2-acrylamidoethoxy)phenylmethylene]-β-D-mannopyranoside
CAS No.:1318073-95-8
Molecular Formula:C₃₉H₃₅NO₁₁
Molecular Weight:693.707
Hs Code.:

Synonyms:3,4,6-tri-O-benzoyl-1,2-O-[(2-acrylamidoethoxy)phenylmethylene]-β-D-mannopyranoside

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Chemical Property of 3,4,6-tri-O-benzoyl-1,2-O-[(2-acrylamidoethoxy)phenylmethylene]-β-D-mannopyranoside

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Technology Process of 3,4,6-tri-O-benzoyl-1,2-O-[(2-acrylamidoethoxy)phenylmethylene]-β-D-mannopyranoside

There total 1 articles about 3,4,6-tri-O-benzoyl-1,2-O-[(2-acrylamidoethoxy)phenylmethylene]-β-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 953795-87-4
3,4,6-tri-O-benzoyl-β-D-mannopyranose-1,2-(prop-2-ynyl orthobenzoate)

: 7646-67-5,28156-60-7
N-hydroxyethylacrylamide

: 1318073-95-8
3,4,6-tri-O-benzoyl-1,2-O-[(2-acrylamidoethoxy)phenylmethylene]-β-D-mannopyranoside

Guidance literature:: With gold(III) tribromide; In dichloromethane; at 20 ℃; for 10h; Inert atmosphere; Molecular sieve;
DOI:10.1016/j.carres.2011.04.018

Reference yield:

: 1318073-95-8
3,4,6-tri-O-benzoyl-1,2-O-[(2-acrylamidoethoxy)phenylmethylene]-β-D-mannopyranoside

: 1318073-99-2
2-(acrylamido)ethyl 2,3,4,6-tetra-O-benzoyl-α-D-mannopyranoside

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In dichloromethane; at 20 ℃; for 0.0833333h;
DOI:10.1016/j.carres.2011.04.018

Reference yield:

: 1318073-95-8
3,4,6-tri-O-benzoyl-1,2-O-[(2-acrylamidoethoxy)phenylmethylene]-β-D-mannopyranoside

: 1318074-12-2
C₄₈H₅₂N₂O₁₅S

Guidance literature:: Multi-step reaction with 2 steps

1: trimethylsilyl trifluoromethanesulfonate / dichloromethane / 0.08 h / 20 °C

2: triethylamine / ethanol / 8 h / 20 °C / Inert atmosphere

With trimethylsilyl trifluoromethanesulfonate; triethylamine; In ethanol; dichloromethane; 2: Michael addition;
DOI:10.1016/j.carres.2011.04.018