2-(S)-t-butoxycarbonylamino-3-[4'-(1''-t-butoxycarbonyl)cyclopropyl]benzenepropanoic acid benzyl ester

Base Information

Chemical Name:2-(S)-t-butoxycarbonylamino-3-[4'-(1''-t-butoxycarbonyl)cyclopropyl]benzenepropanoic acid benzyl ester
CAS No.:228410-34-2
Molecular Formula:C₂₉H₃₇NO₆
Molecular Weight:495.616
Hs Code.:

Synonyms:2-(S)-t-butoxycarbonylamino-3-[4'-(1''-t-butoxycarbonyl)cyclopropyl]benzenepropanoic acid benzyl ester

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Chemical Property of 2-(S)-t-butoxycarbonylamino-3-[4'-(1''-t-butoxycarbonyl)cyclopropyl]benzenepropanoic acid benzyl ester

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Technology Process of 2-(S)-t-butoxycarbonylamino-3-[4'-(1''-t-butoxycarbonyl)cyclopropyl]benzenepropanoic acid benzyl ester

There total 1 articles about 2-(S)-t-butoxycarbonylamino-3-[4'-(1''-t-butoxycarbonyl)cyclopropyl]benzenepropanoic acid benzyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 228410-33-1
tert-butyl 1-(4-iodophenyl)cyclopropane-1-carboxylate

: 108957-20-6
(R)-N-(tert-butoxycarbonyl)-3-iodoalanine benzyl ester

: 228410-34-2
2-(S)-t-butoxycarbonylamino-3-[4'-(1''-t-butoxycarbonyl)cyclopropyl]benzenepropanoic acid benzyl ester

Guidance literature:: With 1,1-Dibromoethane; zinc; In THF (tetrahydrofurane); at 40 ℃; for 0.666667h; Sonication;

(R)-N-(tert-butoxycarbonyl)-3-iodoalanine benzyl ester; In ISOPROPYLAMIDE; at 55 ℃; for 1h;

tert-butyl 1-(4-iodophenyl)cyclopropane-1-carboxylate; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tris-(o-tolyl)phosphine; In ISOPROPYLAMIDE; for 16h; Heating / reflux;

Reference yield: 66.0%

: 228410-34-2
2-(S)-t-butoxycarbonylamino-3-[4'-(1''-t-butoxycarbonyl)cyclopropyl]benzenepropanoic acid benzyl ester

: 228410-35-3
2-(S)-t-butoxycarbonylamino-3-[4'-(1''-t-butoxycarbonyl)cyclopropyl]benzenepropanoic acid

Guidance literature:: 2-(S)-t-butoxycarbonylamino-3-[4'-(1''-t-butoxycarbonyl)cyclopropyl]benzenepropanoic acid benzyl ester; With lithium hydroxide; water; In tetrahydrofuran; at 20 ℃; for 16h;

With potassium hydrogensulfate; In tetrahydrofuran; water;