(S)-3-Phenyl-2-(2,2,2-trifluoro-acetylamino)-propionic acid 2-phenylselanyl-ethyl ester

Base Information

Chemical Name:(S)-3-Phenyl-2-(2,2,2-trifluoro-acetylamino)-propionic acid 2-phenylselanyl-ethyl ester
CAS No.:147092-01-1
Molecular Formula:C₁₉H₁₈F₃NO₃Se
Molecular Weight:444.312
Hs Code.:

Synonyms:(S)-3-Phenyl-2-(2,2,2-trifluoro-acetylamino)-propionic acid 2-phenylselanyl-ethyl ester

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Chemical Property of (S)-3-Phenyl-2-(2,2,2-trifluoro-acetylamino)-propionic acid 2-phenylselanyl-ethyl ester

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Technology Process of (S)-3-Phenyl-2-(2,2,2-trifluoro-acetylamino)-propionic acid 2-phenylselanyl-ethyl ester

There total 1 articles about (S)-3-Phenyl-2-(2,2,2-trifluoro-acetylamino)-propionic acid 2-phenylselanyl-ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 65275-32-3
2-(phenylselenyl)ethanol

: 350-09-4
N-trifluoroacetyl-L-phenylalanine

: 147092-01-1
(S)-3-Phenyl-2-(2,2,2-trifluoro-acetylamino)-propionic acid 2-phenylselanyl-ethyl ester

Guidance literature:: With dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In N,N-dimethyl-formamide; for 12h; Ambient temperature;
DOI:10.1055/s-1993-25802

Reference yield:

: 147092-01-1
(S)-3-Phenyl-2-(2,2,2-trifluoro-acetylamino)-propionic acid 2-phenylselanyl-ethyl ester

: C₁₉H₁₈F₃NO₄Se

Guidance literature:: With dihydrogen peroxide; In tetrahydrofuran; 1.) 0 deg C, 30 min, 2.) r.t., 12 h;
DOI:10.1055/s-1993-25802

Reference yield:

: 147092-01-1
(S)-3-Phenyl-2-(2,2,2-trifluoro-acetylamino)-propionic acid 2-phenylselanyl-ethyl ester

: N-(trifluoroacetyl)phenylalanine vinyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 30percent H₂O₂ / tetrahydrofuran / 1.) 0 deg C, 30 min, 2.) r.t., 12 h

2: CHCl₃ / 12 h / Heating

With dihydrogen peroxide; In tetrahydrofuran; chloroform;
DOI:10.1055/s-1993-25802