12-methoxy-N,N-(tetrachlorophthaloyl)dehydroabietylamine p-tosylhydrazone

Base Information

Chemical Name:12-methoxy-N,N-(tetrachlorophthaloyl)dehydroabietylamine p-tosylhydrazone
CAS No.:1415684-68-2
Molecular Formula:C₃₆H₃₇Cl₄N₃O₅S
Molecular Weight:765.585
Hs Code.:

Synonyms:12-methoxy-N,N-(tetrachlorophthaloyl)dehydroabietylamine p-tosylhydrazone

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Chemical Property of 12-methoxy-N,N-(tetrachlorophthaloyl)dehydroabietylamine p-tosylhydrazone

Chemical Property:

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Technology Process of 12-methoxy-N,N-(tetrachlorophthaloyl)dehydroabietylamine p-tosylhydrazone

There total 8 articles about 12-methoxy-N,N-(tetrachlorophthaloyl)dehydroabietylamine p-tosylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1415684-65-9
12-Methoxy-7-oxo-N,N-(tetrachlorophthaloyl)dehydroabietylamine

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 1415684-68-2
12-methoxy-N,N-(tetrachlorophthaloyl)dehydroabietylamine p-tosylhydrazone

Guidance literature:: With toluene-4-sulfonic acid; In ethanol; benzene; for 8h; Inert atmosphere; Reflux;
DOI:10.1016/j.tet.2012.10.071

Reference yield:

: 1415684-59-1
(4R)-12-acetoxy-N,N-(tetrachlorophthaloyl)dehydroabietylamine

: 1415684-68-2
12-methoxy-N,N-(tetrachlorophthaloyl)dehydroabietylamine p-tosylhydrazone

Guidance literature:: Multi-step reaction with 4 steps

1: chromium(VI) oxide; tert.-butylhydroperoxide / dichloromethane; pyridine / 25 h / 20 °C

2: hydrogenchloride / chloroform; methanol / 1.5 h / Reflux; Inert atmosphere

3: potassium carbonate / acetone / 5 h / Inert atmosphere; Reflux

4: toluene-4-sulfonic acid / benzene; ethanol / 8 h / Inert atmosphere; Reflux

With chromium(VI) oxide; hydrogenchloride; tert.-butylhydroperoxide; potassium carbonate; toluene-4-sulfonic acid; In pyridine; methanol; ethanol; dichloromethane; chloroform; acetone; benzene;
DOI:10.1016/j.tet.2012.10.071

Reference yield:

: 1415684-63-7
12-acetoxy-7-oxo-N,N-(tetrachlorophthaloyl)dehydroabietylamine

: 1415684-68-2
12-methoxy-N,N-(tetrachlorophthaloyl)dehydroabietylamine p-tosylhydrazone

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogenchloride / chloroform; methanol / 1.5 h / Reflux; Inert atmosphere

2: potassium carbonate / acetone / 5 h / Inert atmosphere; Reflux

3: toluene-4-sulfonic acid / benzene; ethanol / 8 h / Inert atmosphere; Reflux

With hydrogenchloride; potassium carbonate; toluene-4-sulfonic acid; In methanol; ethanol; chloroform; acetone; benzene;
DOI:10.1016/j.tet.2012.10.071