4-fluorobenzyl methyl carbonate

Base Information

• Chemical Name: 4-fluorobenzyl methyl carbonate
• CAS No.: 1350846-05-7
• Molecular Formula: C₉H₉FO₃
• Molecular Weight: 184.167

Synonyms:4-fluorobenzyl methyl carbonate

Chemical Property of 4-fluorobenzyl methyl carbonate

Chemical Property:

Purity/Quality:

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Technology Process of 4-fluorobenzyl methyl carbonate

There total 3 articles about 4-fluorobenzyl methyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

4-fluorobenzylic alcohol (459-56-3) + carbonic acid dimethyl ester (616-38-6) → 4-fluorobenzyl methyl carbonate (1350846-05-7)

Guidance literature:

With manganese(II)carbonate; at 90 ℃; for 15h; Green chemistry;

DOI:10.1007/s10562-020-03310-z

Reference yield:

4-fluorobenzylic alcohol (459-56-3) + methyl 1-imidazolecarboxylate (61985-23-7) → 4-fluorobenzyl methyl carbonate (1350846-05-7)

Guidance literature:

In dichloromethane; at 20 ℃; for 48h; Inert atmosphere;

DOI:10.1021/ja2095393

Reference yield:

4-fluorobenzylic alcohol (459-56-3) + methyl chloroformate (79-22-1) → 4-fluorobenzyl methyl carbonate (1350846-05-7)

Guidance literature:

With triethylamine; Inert atmosphere;

DOI:10.1246/cl.170901

upstream raw materials:

4-fluorobenzylic alcohol

methyl 1-imidazolecarboxylate

methyl chloroformate

carbonic acid dimethyl ester

Downstream raw materials:

3-(4-fluorobenzyl)-2,3-dimethyl-3H-indole

p-Fluorophenylacetic acid

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