2-(tetraphen-4-yl)cyclohexanol

Base Information

Chemical Name:2-(tetraphen-4-yl)cyclohexanol
CAS No.:111189-57-2
Molecular Formula:C₂₄H₂₂O
Molecular Weight:326.438
Hs Code.:

Synonyms:2-(4-benzanthracenyl)cyclohexanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-(tetraphen-4-yl)cyclohexanol

Chemical Property:

Vapor Pressure:1.1E-13mmHg at 25°C

Purity/Quality:

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Technology Process of 2-(tetraphen-4-yl)cyclohexanol

There total 3 articles about 2-(tetraphen-4-yl)cyclohexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2498-66-0
benz[a]anthracene-7,12-dione

: 111189-57-2
2-(4-benz anthracenyl)cyclohexanol

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / bromine / acetic acid / 4 h / Heating

2: 1.) hydroiodic acid, hypophosphorous acid, 2.) chloranil / 1.) acetic acid, reflux, 18 h, 2.) benzene, reflux, overnight

3: 1.) n-butyllithium / benzene, hexane, 50 deg C, 1 h, 2.) benzene, hexane, 50 deg C, 5 h

With n-butyllithium; hydrogen iodide; bromine; hypophosphorous acid; chloranil; In acetic acid;
DOI:10.1021/jo00235a005

Reference yield:

: 63715-52-6
4-Bromobenz anthracene-7,12-dione

: 111189-57-2
2-(4-benz anthracenyl)cyclohexanol

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) hydroiodic acid, hypophosphorous acid, 2.) chloranil / 1.) acetic acid, reflux, 18 h, 2.) benzene, reflux, overnight

2: 1.) n-butyllithium / benzene, hexane, 50 deg C, 1 h, 2.) benzene, hexane, 50 deg C, 5 h

With n-butyllithium; hydrogen iodide; hypophosphorous acid; chloranil;
DOI:10.1021/jo00235a005

Reference yield:

: 61921-39-9
4-bromo-benz[a]anthracene

: 286-20-4
cyclohexane-1,2-epoxide

: 111189-57-2
2-(4-benz anthracenyl)cyclohexanol

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction; benzene, hexane, 50 deg C, 1 h, 2.) benzene, hexane, 50 deg C, 5 h;
DOI:10.1021/jo00235a005