methyl 4-(1-cyano-4-hydroxy-7-phenoxyisoquinoline-3-carboxamido)-4-methylpentanoate

Base Information

Chemical Name:methyl 4-(1-cyano-4-hydroxy-7-phenoxyisoquinoline-3-carboxamido)-4-methylpentanoate
CAS No.:1455092-71-3
Molecular Formula:C₂₄H₂₃N₃O₅
Molecular Weight:433.464
Hs Code.:

Synonyms:methyl 4-(1-cyano-4-hydroxy-7-phenoxyisoquinoline-3-carboxamido)-4-methylpentanoate

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Chemical Property of methyl 4-(1-cyano-4-hydroxy-7-phenoxyisoquinoline-3-carboxamido)-4-methylpentanoate

Chemical Property:

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Technology Process of methyl 4-(1-cyano-4-hydroxy-7-phenoxyisoquinoline-3-carboxamido)-4-methylpentanoate

There total 3 articles about methyl 4-(1-cyano-4-hydroxy-7-phenoxyisoquinoline-3-carboxamido)-4-methylpentanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1455095-87-0
methyl 4-amino-4-methylpentanoate acetate

: 1455092-67-7
1-cyano-4-hydroxy-7-phenoxyisoquinoline-3-carboxylic acid

: 1455092-71-3
methyl 4-(1-cyano-4-hydroxy-7-phenoxyisoquinoline-3-carboxamido)-4-methylpentanoate

Guidance literature:: With N-ethylmorpholine;; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 20h;

Reference yield:

: 16507-02-1
methyl 4-methyl-4-nitropentanoate

: 1455092-71-3
methyl 4-(1-cyano-4-hydroxy-7-phenoxyisoquinoline-3-carboxamido)-4-methylpentanoate

Guidance literature:: Multi-step reaction with 2 steps

1: palladium on activated carbon; hydrogen / 16 h / 20 °C

2: N-ethylmorpholine;; dicyclohexyl-carbodiimide; benzotriazol-1-ol / dichloromethane / 20 h / 20 °C

With N-ethylmorpholine;; palladium on activated carbon; hydrogen; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In dichloromethane;

Reference yield:

: 1455091-23-2
1-cyano-4-hydroxy-7-phenoxyisoquinoline-3-carboxylic acid methyl ester

: 1455092-71-3
methyl 4-(1-cyano-4-hydroxy-7-phenoxyisoquinoline-3-carboxamido)-4-methylpentanoate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / methanol; tetrahydrofuran; water / 5 h / 20 °C

2: N-ethylmorpholine;; dicyclohexyl-carbodiimide; benzotriazol-1-ol / dichloromethane / 20 h / 20 °C

With N-ethylmorpholine;; benzotriazol-1-ol; dicyclohexyl-carbodiimide; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water;