di(tert-butyl) (2R,4S)-5-hydroxy-4-methyl-1-phenylpentan-2-yliminodicarbonate

Base Information

Chemical Name:di(tert-butyl) (2R,4S)-5-hydroxy-4-methyl-1-phenylpentan-2-yliminodicarbonate
CAS No.:936691-38-2
Molecular Formula:C₂₂H₃₅NO₅
Molecular Weight:393.524
Hs Code.:

Synonyms:di(tert-butyl) (2R,4S)-5-hydroxy-4-methyl-1-phenylpentan-2-yliminodicarbonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of di(tert-butyl) (2R,4S)-5-hydroxy-4-methyl-1-phenylpentan-2-yliminodicarbonate

Chemical Property:

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Technology Process of di(tert-butyl) (2R,4S)-5-hydroxy-4-methyl-1-phenylpentan-2-yliminodicarbonate

There total 3 articles about di(tert-butyl) (2R,4S)-5-hydroxy-4-methyl-1-phenylpentan-2-yliminodicarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₃₈H₅₃NO₅Si

: 936691-38-2
di(tert-butyl) (2R,4S)-5-hydroxy-4-methyl-1-phenylpentan-2-yliminodicarbonate

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃;
DOI:10.1021/ol070415q

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 936691-38-2
di(tert-butyl) (2R,4S)-5-hydroxy-4-methyl-1-phenylpentan-2-yliminodicarbonate

Guidance literature:: Multi-step reaction with 2 steps

1: butyllithium / tetrahydrofuran; hexane / -78 - 20 °C

2: 0.44 g / tetrabutylammonium fluoride / tetrahydrofuran / 20 °C

With n-butyllithium; tetrabutyl ammonium fluoride; In tetrahydrofuran; hexane;
DOI:10.1021/ol070415q

Reference yield:

: 936691-37-1
[1-benzyl-4-(tert-butyl-diphenyl-silanyloxy)-3-methyl-butyl]-carbamic acid tert-butyl ester

: 936691-38-2
di(tert-butyl) (2R,4S)-5-hydroxy-4-methyl-1-phenylpentan-2-yliminodicarbonate

Guidance literature:: Multi-step reaction with 2 steps

1: butyllithium / tetrahydrofuran; hexane / -78 - 20 °C

2: 0.44 g / tetrabutylammonium fluoride / tetrahydrofuran / 20 °C

With n-butyllithium; tetrabutyl ammonium fluoride; In tetrahydrofuran; hexane;
DOI:10.1021/ol070415q