hex-1-en-5-one 2,4,6-tri-isopropylbenzenesulphonyl hydrazone

Base Information

Chemical Name:hex-1-en-5-one 2,4,6-tri-isopropylbenzenesulphonyl hydrazone
CAS No.:64028-02-0
Molecular Formula:C₂₁H₃₄N₂O₂S
Molecular Weight:378.579
Hs Code.:

Synonyms:hex-1-en-5-one 2,4,6-tri-isopropylbenzenesulphonyl hydrazone

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of hex-1-en-5-one 2,4,6-tri-isopropylbenzenesulphonyl hydrazone

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Technology Process of hex-1-en-5-one 2,4,6-tri-isopropylbenzenesulphonyl hydrazone

There total 3 articles about hex-1-en-5-one 2,4,6-tri-isopropylbenzenesulphonyl hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 109-49-9
5-Hexen-2-one

: 39085-59-1
trisylhydrazine

: 64028-02-0
hex-1-en-5-one 2,4,6-tri-isopropylbenzenesulphonyl hydrazone

Guidance literature:: In tetrahydrofuran; for 2h; Ambient temperature;
DOI:10.1039/P19800001487

Reference yield: 94.0%

: 61835-96-9
acetone-2,4,6-tri-isopropylbenzenesulphonylhydrazone

: 106-95-6
allyl bromide

: 64028-02-0
hex-1-en-5-one 2,4,6-tri-isopropylbenzenesulphonyl hydrazone

Guidance literature:: With n-butyllithium; In 1,2-dimethoxyethane; at -65 ℃; for 1h;
DOI:10.1039/P19810002848

Reference yield:

: 39085-59-1
trisylhydrazine

: 64028-02-0
hex-1-en-5-one 2,4,6-tri-isopropylbenzenesulphonyl hydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: 92 percent / 0.42 h

2: 94 percent / n-butyl-lithium / 1,2-dimethoxy-ethane / 1 h / -65 °C

With n-butyllithium; In 1,2-dimethoxyethane;
DOI:10.1039/P19810002848