5'-O-1,1-bis(tert-butyl)[(pyren-1-yl)methoxy]silyl-N⁶-benzoyl deoxyadenosine

Base Information

Chemical Name:5'-O-1,1-bis(tert-butyl)[(pyren-1-yl)methoxy]silyl-N⁶-benzoyl deoxyadenosine
CAS No.:945623-54-1
Molecular Formula:C₄₂H₄₅N₅O₅Si
Molecular Weight:727.935
Hs Code.:

5'-O-1,1-bis(tert-butyl)[(pyren-1-yl)methoxy]silyl-N<sup>6</sup>-benzoyl deoxyadenosine

Synonyms:5'-O-1,1-bis(tert-butyl)[(pyren-1-yl)methoxy]silyl-N⁶-benzoyl deoxyadenosine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5'-O-1,1-bis(tert-butyl)[(pyren-1-yl)methoxy]silyl-N⁶-benzoyl deoxyadenosine

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Technology Process of 5'-O-1,1-bis(tert-butyl)[(pyren-1-yl)methoxy]silyl-N⁶-benzoyl deoxyadenosine

There total 3 articles about 5'-O-1,1-bis(tert-butyl)[(pyren-1-yl)methoxy]silyl-N⁶-benzoyl deoxyadenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 912558-79-3
1,1-bis(tert-butyl)[(pyren-1-yl)methoxy]silyl chloride

: 4546-72-9
N₆-benzoyl-2'-deoxyadenosine

: 945623-54-1
5'-O-1,1-bis(tert-butyl)[(pyren-1-yl)methoxy]silyl-N⁶-benzoyl deoxyadenosine

Guidance literature:: With dmap; TEA; In pyridine; for 16h;
DOI:10.1246/cl.2007.768

Reference yield:

: 18395-90-9
Di-tert-butyldichlorosilane

: 945623-54-1
5'-O-1,1-bis(tert-butyl)[(pyren-1-yl)methoxy]silyl-N⁶-benzoyl deoxyadenosine

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / NaOH / pyridine; methanol / 2 h / 20 °C

2: 89 percent / DMAP; TEA / pyridine / 16 h

With dmap; sodium hydroxide; TEA; In pyridine; methanol;
DOI:10.1246/cl.2007.768

Reference yield:

: 24463-15-8
1-pyrenemethanol

: 945623-54-1
5'-O-1,1-bis(tert-butyl)[(pyren-1-yl)methoxy]silyl-N⁶-benzoyl deoxyadenosine

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / NaOH / pyridine; methanol / 2 h / 20 °C

2: 89 percent / DMAP; TEA / pyridine / 16 h

With dmap; sodium hydroxide; TEA; In pyridine; methanol;
DOI:10.1246/cl.2007.768