C₃₄H₄₆O₁₂

Base Information

Chemical Name:C₃₄H₄₆O₁₂
CAS No.:1018988-66-3
Molecular Formula:C₃₄H₄₆O₁₂
Molecular Weight:646.732
Hs Code.:

C<sub>34</sub>H<sub>46</sub>O<sub>12</sub>

Synonyms:C₃₄H₄₆O₁₂

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Chemical Property of C₃₄H₄₆O₁₂

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Technology Process of C₃₄H₄₆O₁₂

There total 19 articles about C₃₄H₄₆O₁₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1018988-51-6
C₅₀H₆₄O₁₂Si

: 1018988-66-3
C₃₄H₄₆O₁₂

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 0 ℃; for 2h; Inert atmosphere;
DOI:10.1002/asia.200800429

Reference yield: 88.0%

: 1018988-54-9
C₃₄H₄₄O₁₂

: 1018988-66-3
C₃₄H₄₆O₁₂

Guidance literature:: With sodium tetrahydroborate; In methanol; at 0 ℃; for 0.5h;
DOI:10.1002/anie.200704959

Reference yield:

: 1018988-60-7
C₅₈H₇₈O₇Si₃

: 1018988-66-3
C₃₄H₄₆O₁₂

Guidance literature:: Multi-step reaction with 12 steps

1.1: 2,6-di-tert-butyl-4-methylpyridine; 2,3-dicyano-5,6-dichloro-p-benzoquinone / acetonitrile / 20 °C / Inert atmosphere

2.1: sodium tetrahydroborate / tetrahydrofuran; ethanol / -40 - -30 °C / Inert atmosphere

3.1: sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 24 h / 13 °C / Inert atmosphere

4.1: lithium borohydride / tetrahydrofuran / Inert atmosphere; Reflux

4.2: 4 h / 20 °C / Inert atmosphere

5.1: lithium borohydride / tetrahydrofuran / 26.5 h / 20 °C / Inert atmosphere; Reflux

5.2: 4 h / 20 °C / Inert atmosphere

6.1: water; acetic acid / tetrahydrofuran / 2 h / 20 °C / Inert atmosphere

7.1: dmap / pyridine; dichloromethane / 24 h / 20 °C / Inert atmosphere

8.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 0 °C / Inert atmosphere

9.1: peracetic acid; mercury(II) diacetate; acetic acid / 4 h / 20 °C / Inert atmosphere

10.1: 1H-imidazole / dichloromethane / 4 h / 0 °C / Inert atmosphere

11.1: dmap / pyridine; dichloromethane / 0 - 40 °C / Inert atmosphere

12.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 2 h / 0 °C / Inert atmosphere

With 1H-imidazole; peracetic acid; dmap; sodium tetrahydroborate; lithium borohydride; 2,6-di-tert-butyl-4-methylpyridine; mercury(II) diacetate; tetrabutyl ammonium fluoride; water; sodium hydrogencarbonate; acetic acid; 3-chloro-benzenecarboperoxoic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; pyridine; ethanol; dichloromethane; acetonitrile; 2.1: Luche reduction / 9.1: Tamao oxidation;
DOI:10.1002/asia.200800429