(+)-1-(benzyloxycarbonyl)-2(R)-tert-butyl-3-<(S)-methyl(methoxycarbonyl)methyl>imidazolidin-4-one

Base Information

Chemical Name:(+)-1-(benzyloxycarbonyl)-2(R)-tert-butyl-3-<(S)-methyl(methoxycarbonyl)methyl>imidazolidin-4-one
CAS No.:115572-68-4
Molecular Formula:C₁₉H₂₆N₂O₅
Molecular Weight:362.426
Hs Code.:

Synonyms:(+)-1-(benzyloxycarbonyl)-2(R)-tert-butyl-3-<(S)-methyl(methoxycarbonyl)methyl>imidazolidin-4-one

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+)-1-(benzyloxycarbonyl)-2(R)-tert-butyl-3-<(S)-methyl(methoxycarbonyl)methyl>imidazolidin-4-one

Chemical Property:

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Technology Process of (+)-1-(benzyloxycarbonyl)-2(R)-tert-butyl-3-<(S)-methyl(methoxycarbonyl)methyl>imidazolidin-4-one

There total 1 articles about (+)-1-(benzyloxycarbonyl)-2(R)-tert-butyl-3-<(S)-methyl(methoxycarbonyl)methyl>imidazolidin-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 115572-64-0
(S)-2-{2-[2,2-Dimethyl-prop-(E)-ylideneamino]-acetylamino}-propionic acid methyl ester

: 501-53-1,94274-21-2
benzyl chloroformate

: 115572-69-5
(-)-1-(benzyloxycarbonyl)-2(S)-tert-butyl-3-<(S)-methyl(methoxycarbonyl)methyl>imidazolidin-4-one

: 115572-68-4
(+)-1-(benzyloxycarbonyl)-2(R)-tert-butyl-3-<(S)-methyl(methoxycarbonyl)methyl>imidazolidin-4-one

Guidance literature:: With dmap; triethylamine; acetyl chloride; Yield given. Multistep reaction. Yields of byproduct given; 1.) MeOH, room temp., 16 h, 2.) CH₂Cl₂, room temp., overnight;
DOI:10.1021/ja00189a042

Reference yield:

: 115572-68-4
(+)-1-(benzyloxycarbonyl)-2(R)-tert-butyl-3-<(S)-methyl(methoxycarbonyl)methyl>imidazolidin-4-one

: 115572-83-3
(2R,5R)-2-tert-Butyl-3-((R)-1-carboxy-ethyl)-5-methyl-4-oxo-imidazolidine-1-carboxylic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

2: NaOH / methanol

With sodium hydroxide; In methanol;
DOI:10.1002/hlca.19870700727

Reference yield:

: 115572-68-4
(+)-1-(benzyloxycarbonyl)-2(R)-tert-butyl-3-<(S)-methyl(methoxycarbonyl)methyl>imidazolidin-4-one

: 115572-84-4
1-(benzyloxycarbonyl)-2(R)-tert-butyl-3-(methoxy-(S)-alanyl-(R)-alanyl)-5(R)-imidazolidin-4-one

Guidance literature:: Multi-step reaction with 3 steps

2: NaOH / methanol

3: DCC/HOBT

With sodium hydroxide; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In methanol;
DOI:10.1002/hlca.19870700727